METHANE-D3-THIOL

Base Information

• Chemical Name: METHANE-D3-THIOL
• CAS No.: 7175-74-8
• Molecular Formula: CH₄S
• Molecular Weight: 51.0849
• Mol file: 7175-74-8.mol

Synonyms:1,1,1-Trideuteromethanethiol;Methyl-d3 mercaptan

Chemical Property of METHANE-D3-THIOL

Chemical Property:

• Vapor Pressure: 1900mmHg at 25°C
• Flash Point: -18 °C
• PSA: 38.80000
• Density: 0.865g/cm³
• LogP: 0.54600

Purity/Quality:

99% ^*data from raw suppliers

Methane-d3-thiol 98 atom % D ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F+,T,N
• Hazard Codes: F+,T,N
• Statements: 12-23-50/53
• Safety Statements: 16-25-60-61

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHANE-D3-THIOL

There total 3 articles about METHANE-D3-THIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

S-trideuteromethylisothiouronium iodide → trideuteromethanethiol (7175-74-8)

Guidance literature:

With sodium hydroxide; In water;

DOI:10.1080/10426507.2011.615771

Reference yield:

PhCH(OH)C(O)SCD3 (922498-88-2) → trideuteromethanethiol (7175-74-8) + hydroxyphenylacetate (769-61-9)

Guidance literature:

With [(bpta)Zn(CH₃CN)2(H₂O)](ClO₄)2; water; In acetonitrile; at 56.34 ℃; for 288h; pH=9; Reagent/catalyst; Temperature; pH-value; Concentration; Kinetics; aq. buffer;

DOI:10.1021/ic902322h

Reference yield:

→ trideuteromethanethiol (7175-74-8)

Guidance literature:

Thioharnstoff, 1. CD3I, Aceton, Erhitzen (-> Thiuroniumsalz), 2. Anilin, 125 - 155grad;

DOI:10.1021/ja00819a033

upstream raw materials:

PhCH(OH)C(O)SCD₃

Downstream raw materials:

methyl 4-[(trideuteromethylthio)thiocarbonyl]benzoate