1,3-Dithiole, 4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]-

Base Information

Chemical Name:1,3-Dithiole, 4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]-
CAS No.:600718-01-2
Molecular Formula:C63H59N3O6S6
Molecular Weight:1146.57
Hs Code.:

1,3-Dithiole,
4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl
methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]-

Synonyms:

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Chemical Property of 1,3-Dithiole, 4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]-

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Technology Process of 1,3-Dithiole, 4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]-

There total 4 articles about 1,3-Dithiole, 4-[[[4-(azidomethyl)cyclohexyl]methyl]thio]-2-[4-[[[3,5-bis[[3,5-bis(phenyl methoxy)phenyl]methoxy]phenyl]methyl]thio]-1,3-dithiol-2-ylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 791100-63-5
3-[(E)-4'-(2-Cyano-ethylsulfanyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-propionitrile

: 600718-01-2
(E)-4'-(4-Azidomethyl-cyclohexylmethylsulfanyl)-4-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 5 steps

1: CsOH*H₂O / tetrahydrofuran; methanol / 1 h / 20 °C

2: tetrahydrofuran; methanol / 20 °C

3: CsOH*H₂O / tetrahydrofuran; methanol / 1 h / 20 °C

4: tetrahydrofuran; methanol / 20 °C

5: 73 percent / NaN₃ / dimethylformamide / 25 - 80 °C

With cesium hydroxide; sodium azide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00700-2

Reference yield:

: Caesium; (E)-4'-(2-cyano-ethylsulfanyl)-[2,2']bi[[1,3]dithiolylidene]-4-thiolate

: 600718-01-2
(E)-4'-(4-Azidomethyl-cyclohexylmethylsulfanyl)-4-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; methanol / 20 °C

2: CsOH*H₂O / tetrahydrofuran; methanol / 1 h / 20 °C

3: tetrahydrofuran; methanol / 20 °C

4: 73 percent / NaN₃ / dimethylformamide / 25 - 80 °C

With cesium hydroxide; sodium azide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00700-2

Reference yield:

: 600717-99-5
3-{(E)-4'-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propionitrile

: 600718-01-2
(E)-4'-(4-Azidomethyl-cyclohexylmethylsulfanyl)-4-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 3 steps

1: CsOH*H₂O / tetrahydrofuran; methanol / 1 h / 20 °C

2: tetrahydrofuran; methanol / 20 °C

3: 73 percent / NaN₃ / dimethylformamide / 25 - 80 °C

With cesium hydroxide; sodium azide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00700-2