Propanedioic acid, [(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3- benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester

Base Information

Chemical Name:Propanedioic acid, [(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3- benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester
CAS No.:600725-53-9
Molecular Formula:C34H45N3O6
Molecular Weight:591.748
Hs Code.:

Propanedioic acid,
[(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3-
benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanedioic acid, [(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3- benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester

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Technology Process of Propanedioic acid, [(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3- benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester

There total 1 articles about Propanedioic acid, [(3,4-diethylphenyl)methyl][2-oxo-2-[4-(1,2,4,5-tetrahydro-2-oxo-3H-1,3- benzodiazepin-3-yl)-1-piperidinyl]ethyl]-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 291509-61-0
3-(4-piperidinyl)-1,3,4,5-tetrahydro-1,3-benzodiazepin-2-one

: 600725-52-8
4-(3,4-diethyl-phenyl)-3,3-bis-ethoxycarbonyl-butanoic acid

: 600725-53-9
diethyl-2-(3,4-diethyl-benzyl)-2-{2-oxo-2-[4-(2-oxo-1,2,4,5-tetrahydro-1,3-benzodiazepin-3-yl)-piperidin-1-yl]-ethyl}-malonate

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 5h;

Reference yield: 94.0%

: 600725-53-9
diethyl-2-(3,4-diethyl-benzyl)-2-{2-oxo-2-[4-(2-oxo-1,2,4,5-tetrahydro-1,3-benzodiazepin-3-yl)-piperidin-1-yl]-ethyl}-malonate

: 600725-54-0
2-(3,4-diethyl-benzyl)-4-oxo-4-[4-(2-oxo-1,2,4,5-tetrahydro-1,3-benzodiazepin-3-yl)-piperidin-1-yl]-butyric acid

Guidance literature:: diethyl-2-(3,4-diethyl-benzyl)-2-{2-oxo-2-[4-(2-oxo-1,2,4,5-tetrahydro-1,3-benzodiazepin-3-yl)-piperidin-1-yl]-ethyl}-malonate; With potassium hydroxide; In ethanol; water; for 16h; Heating / reflux;

With hydrogenchloride; In water; at 20 ℃; for 1h; pH=4;