Benzonitrile, 2-bromo-3-methyl-5-(octyloxy)-

Base Information

Chemical Name:Benzonitrile, 2-bromo-3-methyl-5-(octyloxy)-
CAS No.:601479-05-4
Molecular Formula:C16H22BrNO
Molecular Weight:324.261
Hs Code.:

Synonyms:

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Chemical Property of Benzonitrile, 2-bromo-3-methyl-5-(octyloxy)-

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Technology Process of Benzonitrile, 2-bromo-3-methyl-5-(octyloxy)-

There total 6 articles about Benzonitrile, 2-bromo-3-methyl-5-(octyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 601478-98-2
2-bromo-3-methyl-5-octyloxybenzylamine

: 601479-05-4
1-bromo-2-cyano-6-methyl-4-octyloxybenzene

Guidance literature:: With pyridine; oxygen; copper(l) chloride; 4 A molecular sieve; at 60 ℃; for 34h;
DOI:10.1021/jo034652s

Reference yield:

: 7463-51-6
4-bromo-3,5-dimethylphenol

: 601479-05-4
1-bromo-2-cyano-6-methyl-4-octyloxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 91 percent / anhydrous potassium carbonate / ethanol / 24 h / Heating

2.1: 47 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄; H₂O / 5 h / Irradiation; heating

3.1: hexamethylenetetramine / CH₂Cl₂ / Heating

3.2: 45 percent / hydrochloric acid / ethanol; H₂O / 1 h

4.1: 80 percent / oxygen; copper(I) chloride; pyridine / molecular sieves 4 Angstroem / 34 h / 60 °C

With pyridine; N-Bromosuccinimide; hexamethylenetetramine; oxygen; potassium carbonate; copper(l) chloride; dibenzoyl peroxide; 4 A molecular sieve; In tetrachloromethane; ethanol; dichloromethane; water;
DOI:10.1021/jo034652s

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 601479-05-4
1-bromo-2-cyano-6-methyl-4-octyloxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromine; acetic acid

2.1: 91 percent / anhydrous potassium carbonate / ethanol / 24 h / Heating

3.1: 47 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄; H₂O / 5 h / Irradiation; heating

4.1: hexamethylenetetramine / CH₂Cl₂ / Heating

4.2: 45 percent / hydrochloric acid / ethanol; H₂O / 1 h

5.1: 80 percent / oxygen; copper(I) chloride; pyridine / molecular sieves 4 Angstroem / 34 h / 60 °C

With pyridine; N-Bromosuccinimide; hexamethylenetetramine; bromine; oxygen; potassium carbonate; acetic acid; copper(l) chloride; dibenzoyl peroxide; 4 A molecular sieve; In tetrachloromethane; ethanol; dichloromethane; water;
DOI:10.1021/jo034652s