Ethyl phenyl phosphorodithiote

Base Information

• Chemical Name: Ethyl phenyl phosphorodithiote
• CAS No.: 947-34-2
• Molecular Formula: C₁₀H₁₅O₂PS₂
• Molecular Weight: 262.334
• DSSTox Substance ID: DTXSID80241570
• Wikidata: Q83125086
• Mol file: 947-34-2.mol

Synonyms:Ethyl phenyl phosphorodithiote;947-34-2;Phosphorodithioic acid, O,O-diethyl S-phenyl ester;SCHEMBL6073023;DTXSID80241570

Chemical Property of Ethyl phenyl phosphorodithiote

Chemical Property:

• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 262.02510906
• Heavy Atom Count: 15
• Complexity: 208

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOP(=S)(OCC)SC1=CC=CC=C1

Technology Process of Ethyl phenyl phosphorodithiote

There total 13 articles about Ethyl phenyl phosphorodithiote which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

O,O-diethyl S-phenyl phosphorothioate (1889-58-3) → O,O-diethyl S-phenyl phosphorodithioate (947-34-2)

Guidance literature:

With 1,3-dithia-2,4-diphosphetane-2,4-disulfides; In xylene; for 3h; Heating;

Reference yield: 90.0%

diethyl dithiophosphate ammonium salt (1068-22-0) + benzenediazonium tetrafluoroborate (369-57-3) → O,O-diethyl S-phenyl phosphorodithioate (947-34-2)

Guidance literature:

With copper(I) thiocyanate; In acetonitrile; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1002/adsc.201701549

Reference yield: 45.0%

benzenediazonium tetrafluoroborate (369-57-3) + potassium O,O-diethyldithiophosphate (3454-66-8) → O,O-diethyl S-phenyl phosphorodithioate (947-34-2)

Guidance literature:

In water; acetone; at -5 - 0 ℃; for 1h;

upstream raw materials:

benzene diazonium chloride

potassium O,O-diethyldithiophosphate

bis(diethoxyphosphoryl)disulphide

potassium thiophenolate