Carbamic acid, [(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy) propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy) propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl ester
CAS No.:603127-08-8
Molecular Formula:C35H63NO8
Molecular Weight:625.887
Hs Code.:

Carbamic acid,
[(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy)
propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl
ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy) propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy) propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl ester

There total 6 articles about Carbamic acid, [(1S,12S)-1-[(1R,2R)-3-hydroxy-1-(methoxymethoxy)-2-(phenylmethoxy) propyl]-12-(methoxymethoxy)-14-methylpentadecyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 603127-02-2
(3S,4R,5S)-3-Benzyloxy-4-methoxymethoxy-5-((S)-11-methoxymethoxy-13-methyl-tetradecyl)-2-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

: 603127-08-8
[(1S,12S)-1-((1R,2R)-2-Benzyloxy-3-hydroxy-1-methoxymethoxy-propyl)-12-methoxymethoxy-14-methyl-pentadecyl]-carbamic acid tert-butyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol;
DOI:10.1016/S0040-4039(02)02743-0

Reference yield:

: (S)-11-Methoxymethoxy-13-methyl-tetradec-1-yne

: 603127-08-8
[(1S,12S)-1-((1R,2R)-2-Benzyloxy-3-hydroxy-1-methoxymethoxy-propyl)-12-methoxymethoxy-14-methyl-pentadecyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: BuLi / tetrahydrofuran / -78 - 0 °C

1.2: PCC; 4 A MS / CH₂Cl₂

2.1: CAN / acetonitrile; H₂O

2.2: DMAP; Et₃N / CH₂Cl₂

3.1: 95 percent / HCOOH; methanol / Pd

4.1: 74 percent / Ag₂O / ethyl acetate

5.1: 100 percent / (i-Pr)2NEt / CH₂Cl₂

6.1: 100 percent / NaBH₄ / methanol

With methanol; sodium tetrahydroborate; n-butyllithium; formic acid; ammonium cerium(IV) nitrate; N-ethyl-N,N-diisopropylamine; silver(l) oxide; palladium; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4039(02)02743-0

Reference yield:

: 603127-06-6
(2S,3R,4S)-3,4-Bis-benzyloxy-2-((S)-11-methoxymethoxy-13-methyl-tetradec-1-ynyl)-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

: 603127-08-8
[(1S,12S)-1-((1R,2R)-2-Benzyloxy-3-hydroxy-1-methoxymethoxy-propyl)-12-methoxymethoxy-14-methyl-pentadecyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / HCOOH; methanol / Pd

2: 74 percent / Ag₂O / ethyl acetate

3: 100 percent / (i-Pr)2NEt / CH₂Cl₂

4: 100 percent / NaBH₄ / methanol

With methanol; sodium tetrahydroborate; formic acid; N-ethyl-N,N-diisopropylamine; silver(l) oxide; palladium; In methanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4039(02)02743-0