Phosphonic acid, 1-cyclohexen-1-yl-, bis(1-methylethyl) ester

Base Information

Chemical Name:Phosphonic acid, 1-cyclohexen-1-yl-, bis(1-methylethyl) ester
CAS No.:60324-15-4
Molecular Formula:C12H23O3P
Molecular Weight:246.287
Hs Code.:

Synonyms:

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Chemical Property of Phosphonic acid, 1-cyclohexen-1-yl-, bis(1-methylethyl) ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphonic acid, 1-cyclohexen-1-yl-, bis(1-methylethyl) ester

There total 7 articles about Phosphonic acid, 1-cyclohexen-1-yl-, bis(1-methylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 2044-08-8
1-bromocyclohex-1-ene

: 1809-20-7
diisopropyl hydrogenphosphonate

: 60324-15-4
diisopropyl cyclohex-1-enylphosphonate

Guidance literature:: With copper(l) iodide; potassium carbonate; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 110 ℃; for 20h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.202100456

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 60324-15-4
diisopropyl cyclohex-1-enylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenyl phosphite; bromine; triethylamine / dichloromethane / 20 h / -60 °C / Inert atmosphere

1.2: 2 h / Reflux; Inert atmosphere

2.1: copper(l) iodide; sodium iodide; potassium carbonate; N,N`-dimethylethylenediamine / 1,4-dioxane / 20 h / 110 °C / Inert atmosphere; Schlenk technique

With triphenyl phosphite; copper(l) iodide; bromine; potassium carbonate; triethylamine; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; dichloromethane;
DOI:10.1002/ejoc.202100456

Reference yield:

: 116-17-6
triisopropyl phosphite

: 60324-15-4
diisopropyl cyclohex-1-enylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: water / tetrahydrofuran / 48 h / 0 °C / Inert atmosphere

2: copper(l) iodide; sodium iodide; potassium carbonate; N,N`-dimethylethylenediamine / 1,4-dioxane / 20 h / 110 °C / Inert atmosphere; Schlenk technique

With copper(l) iodide; water; potassium carbonate; sodium iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/ejoc.202100456