(2S)-2-(broMoMethyl)-1-Methyl-Pyrrolidine

Base Information

• Chemical Name: (2S)-2-(broMoMethyl)-1-Methyl-Pyrrolidine
• CAS No.: 60365-88-0
• Molecular Formula: C6H12BrN
• Molecular Weight: 178.072
• Mol file: 60365-88-0.mol

Synonyms:2-Bromomethyl-1-methyl-pyrrolidine;(2S)-2-(bromomethyl)-1-methyl-Pyrrolidine;(S)-2-(Bromomethyl)-1-methylpyrrolidine;

Chemical Property of (2S)-2-(broMoMethyl)-1-Methyl-Pyrrolidine

Chemical Property:

• Boiling Point: 179.0±13.0 °C(Predicted)
• PKA: 9.26±0.40(Predicted)
• PSA: 3.24000
• Density: 1.328±0.06 g/cm3(Predicted)
• LogP: 1.41340
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

99%, ^*data from raw suppliers

(S)-2-(Bromomethyl)-1-methylpyrrolidine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2S)-2-(broMoMethyl)-1-Methyl-Pyrrolidine

There total 1 articles about (2S)-2-(broMoMethyl)-1-Methyl-Pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-hydroxymethyl-1-methylpyrrolidine (34381-71-0) → (S)-2-(bromomethyl)-1-methylpyrrolidine (60365-88-0,734470-67-8)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 55.0%

(S)-2-(bromomethyl)-1-methylpyrrolidine (60365-88-0,734470-67-8) + 4-(4-((benzyloxy)carbonyl)piperazin-1-yl)-2-oxo-2,5,6,8-tetrahydropyrido[3,4-d]pyrimidin-7(1H)-carboxylic acid tert-butyl ester → (S)-4-(4-((benzyloxy)carbonyl)piperazin-1-yl)-1-((1-methylpyrrolidin-2-yl)methyl)-2-oxo-2,5,6,8-tetrahydropyrido[3,4-d]pyrimidin-7(1H)-carboxylic acid tert-butyl ester

Guidance literature:

With copper(l) iodide; caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 20h; Sealed tube;

upstream raw materials:

(S)-2-hydroxymethyl-1-methylpyrrolidine

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