5-chloro-2-ethoxybenzoyl chloride

Base Information

• Chemical Name: 5-chloro-2-ethoxybenzoyl chloride
• CAS No.: 60531-34-2
• Molecular Formula: C9H8Cl2O2
• Molecular Weight: 219.067
• Mol file: 60531-34-2.mol

Synonyms:5-Chloro-2-ethoxy-benzoyl chloride;5-chloro-2-ethoxybenzoyl chloride;2-ethoxy-5-chloro-benzoylchloride;2-ethoxy-5-chlorobenzoyl chloride;

Chemical Property of 5-chloro-2-ethoxybenzoyl chloride

Chemical Property:

• PSA: 26.30000
• LogP: 3.11770

Purity/Quality:

98%min ^*data from raw suppliers

5-CHLORO-2-ETHOXYBENZOYLCHLORIDE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-chloro-2-ethoxybenzoyl chloride

There total 2 articles about 5-chloro-2-ethoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-2-ethoxybenzoic acid (62871-12-9) → 5-chloro-2-ethoxybenzoylchloride (60531-34-2)

Guidance literature:

With thionyl chloride; for 2h; Heating / reflux;

Reference yield:

5-bromo-2-ethoxy-benzoic acid (60783-90-6) → 5-chloro-2-ethoxybenzoylchloride (60531-34-2)

Guidance literature:

With thionyl chloride; for 2h; Heating / reflux;

Reference yield: 60.0%

tert-butyl N-[4-({5-[2-(dimethylamino)ethyl]-1-methyl-3-oxo-2-phenylpyrazol-4-yl}amino)-2,2-bis(fluoromethyl)-4-oxobutyl]carbamate + 5-chloro-2-ethoxybenzoylchloride (60531-34-2) → 5-chloro-N-[4-({5-[2-(dimethylamino)ethyl]-1-methyl-3-oxo-2-phenylpyrazol-4-yl}amino)-2,2-bis(fluoromethyl)-4-oxobutyl]-2-ethoxybenzamide

Guidance literature:

tert-butyl N-[4-({5-[2-(dimethylamino)ethyl]-1-methyl-3-oxo-2-phenylpyrazol-4-yl}amino)-2,2-bis(fluoromethyl)-4-oxobutyl]carbamate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.5h;

5-chloro-2-ethoxybenzoylchloride; With triethylamine; In dichloromethane; for 1h;

upstream raw materials:

5-chloro-2-ethoxybenzoic acid

5-bromo-2-ethoxy-benzoic acid

Downstream raw materials:

β-[4-(2-ethoxy-5-chlorobenzamido)-phenyl]-propionic acid

4-(2-<2-ethoxy-5-chloro-benzamido>-ethyl)-benzoic acid

ethyl 4-(2-ethoxy-5-chlorobenzamido)-phenylacetate

{4-[2-(5-Chloro-2-ethoxy-benzoylamino)-ethyl]-phenyl}-acetic acid

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