5-Chloro-2,4-dinitrobenzamide

Base Information

Chemical Name:5-Chloro-2,4-dinitrobenzamide
CAS No.:60532-50-5
Molecular Formula:C7H4ClN3O5
Molecular Weight:245.579
Hs Code.:
DSSTox Substance ID:DTXSID20565106
Wikidata:Q82450046

Synonyms:5-chloro-2,4-dinitrobenzamide;60532-50-5;2,4-Dinitro-5-chlorobenzamide;SCHEMBL3422244;DTXSID20565106;RJJFURIZOMAQLI-UHFFFAOYSA-N

Suppliers and Price of 5-Chloro-2,4-dinitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 5-Chloro-2,4-dinitrobenzamide

Chemical Property:

Melting Point:201-203 °C
Boiling Point:348.1±42.0 °C(Predicted)
PSA：135.72000
Density:1.708±0.06 g/cm3(Predicted)
LogP:3.18590
XLogP3:0.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:244.9839479
Heavy Atom Count:16
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CC(=C1Cl)[N+](=O)[O-])[N+](=O)[O-])C(=O)N

Technology Process of 5-Chloro-2,4-dinitrobenzamide

There total 3 articles about 5-Chloro-2,4-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50425-06-4
5-chloro-2,4-dinitrobenzoyl chloride

: 60532-50-5
5-chloro-2,4-dinitrobenzamide

Guidance literature:: With ammonium hydroxide; at 0 ℃; for 0.5h;
DOI:10.1021/jm000081+

Reference yield:

: 136833-36-8
5-chloro-2,4-dinitrobenzoic acid

: 60532-50-5
5-chloro-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 4 h / Heating

2: conc. aq. NH₄OH / 0.5 h / 0 °C

With ammonium hydroxide; thionyl chloride; In N,N-dimethyl-formamide; 1: Chlorination / 2: Substitution;
DOI:10.1021/jm000081+

Reference yield:

: 535-80-8
3-chlorobenzoate

: 60532-50-5
5-chloro-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / conc. H₂SO₄; KNO₃ / 1.08 h / 40 - 145 °C

2: SOCl₂ / dimethylformamide / 4 h / Heating

3: conc. aq. NH₄OH / 0.5 h / 0 °C

With ammonium hydroxide; thionyl chloride; sulfuric acid; potassium nitrate; In N,N-dimethyl-formamide; 1: Nitration / 2: Chlorination / 3: Substitution;
DOI:10.1021/jm000081+