4ALPHA-METHYL-1,2,3,4,9,10-HEXAHYDROPHENANTHRENE

Base Information

• Chemical Name: 4ALPHA-METHYL-1,2,3,4,9,10-HEXAHYDROPHENANTHRENE
• CAS No.: 60795-82-6
• Molecular Formula: C15H20
• Molecular Weight: 200.324
• Hs Code.: 2902909090
• Mol file: 60795-82-6.mol

Synonyms:4a-Methyl-1,2,3,4,4a,9,10,10a-octahydrophenanthren;4a-Methyl-1,2,3,4,4a,9,10,11-octahydrophenanthren;4a-methyl-1.2.3.4.4a.9.10.10a-octahydro-phenanthrene;4alpha-Methyl-1,2,3,4,4,9,10,-hexahydrophenanthrene;phenanthrene,1,2,3,4,4a,9,10,10a-octahydro-4a-methyl;4b,5,6,7,8,8a,9,10-Oktahydro-4b-methyl-phenanthren;

Chemical Property of 4ALPHA-METHYL-1,2,3,4,9,10-HEXAHYDROPHENANTHRENE

Chemical Property:

• PSA: 0.00000
• LogP: 4.08070

Purity/Quality:

99% ^*data from raw suppliers

4-ALPHA-METHYL-1,2,3,4,9,10,-HEXAHYDROPHENANTHRENE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4ALPHA-METHYL-1,2,3,4,9,10-HEXAHYDROPHENANTHRENE

There total 25 articles about 4ALPHA-METHYL-1,2,3,4,9,10-HEXAHYDROPHENANTHRENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4b-Methyl-4b,5-dihydro-phenanthren (22774-10-3) → 4a-methyl-1.2.3.4.4a.9.10.10a-octahydro-phenanthrene (60795-82-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ja01032a018

Reference yield:

4a-methyl-4,4a-dihydro-3H-phenanthren-2-one (58860-95-0,63723-72-8,63723-73-9) → 4a-methyl-1.2.3.4.4a.9.10.10a-octahydro-phenanthrene (60795-82-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄

2: HCl / diethyl ether

3: H₂ / Pd-C / methanol

With hydrogenchloride; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; diethyl ether;

DOI:10.1021/ja01032a018

Reference yield:

cis-7-Hydroxy-4b-methyl-4b,5,6,7-tetrahydro-phenanthren → 4a-methyl-1.2.3.4.4a.9.10.10a-octahydro-phenanthrene (60795-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / diethyl ether

2: H₂ / Pd-C / methanol

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; diethyl ether;

DOI:10.1021/ja01032a018

upstream raw materials:

4a-Methyl-1,2,3,4,4a,10a-hexahydro-9(10H)-phenanthron

2-methyl-2-phenethyl-cyclohexanol

1-methyl-2-phenethyl-cyclohexanol

1-(2-methyl-cyclohexyl)-2-phenyl-ethanol

Downstream raw materials:

phenanthrene