4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-

Base Information

Chemical Name:4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-
CAS No.:109143-19-3
Molecular Formula:C₁₃H₁₄Cl₂N₂O₄
Molecular Weight:333.171
Hs Code.:2932999099
DSSTox Substance ID:DTXSID30148823
Nikkaji Number:J501.107H
Wikidata:Q83014459
Mol file:109143-19-3.mol

Synonyms:109143-19-3;4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-;N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-1-benzofuran-4-amine;4-(Bis(2-chloroethyl)amino)-5-methoxy-2-nitrobenzofuran;CCRIS 4517;BRN 5607499;4-[BIS(2-CHLOROETHYL)AMINO]-5-METHOXY-2-NITROBENZOFURAN;N,N-Bis(2-chloroethyl)-5-methoxy-2-nitro-4-benzofuranamine;DTXSID30148823

Suppliers and Price of 4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-(BIS(2-CHLOROETHYL)AMINO)-5-METHOXY-2-NITROBENZOFURAN 95.00%
5MG
$ 495.81

Total 1 raw suppliers

Chemical Property of 4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-

Chemical Property:

Vapor Pressure:5.6E-08mmHg at 25°C
Boiling Point:441.1°Cat760mmHg
Flash Point:220.5°C
PSA：71.43000
Density:1.411g/cm³
LogP:4.15680
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:332.0330623
Heavy Atom Count:21
Complexity:350

Purity/Quality:: 4-(BIS(2-CHLOROETHYL)AMINO)-5-METHOXY-2-NITROBENZOFURAN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C2=C(C=C1)OC(=C2)[N+](=O)[O-])N(CCCl)CCCl

Technology Process of 4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro-

There total 6 articles about 4-Benzofuranamine, N,N-bis(2-chloroethyl)-5-methoxy-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 109143-14-8
(N,N-dihydroxyethylamino)-4 methoxy-5 nitro-2 benzofuranne

: 109143-19-3
(N,N-dichlorethylamino)-4 methoxy-5 nitro-2 benzofuranne

Guidance literature:: With trichlorophosphate; for 0.5h; Heating;

Reference yield:

: 82607-27-0
acetyl-4 methoxy-5 nitro-2 benzofuranne

: 109143-19-3
(N,N-dichlorethylamino)-4 methoxy-5 nitro-2 benzofuranne

Guidance literature:: Multi-step reaction with 6 steps

1: 57 percent / K₂CO₃ / aq. ethanol / 4 h / Heating

2: 92 percent / TFA / 4 h / Heating

3: 92 percent / HCl / ethanol / 1 h / Heating

4: 43 percent / 0.17 h / Heating

5: 95 percent / diborane / tetrahydrofuran / 1.5 h / Heating

6: 97 percent / POCl₃ / 0.5 h / Heating

With hydrogenchloride; potassium carbonate; trifluoroacetic acid; diborane; trichlorophosphate; In tetrahydrofuran; ethanol;

Reference yield:

: 109143-03-5
amino-4 methoxy-5 nitro-2 benzofuranne

: 109143-19-3
(N,N-dichlorethylamino)-4 methoxy-5 nitro-2 benzofuranne

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / 0.17 h / Heating

2: 95 percent / diborane / tetrahydrofuran / 1.5 h / Heating

3: 97 percent / POCl₃ / 0.5 h / Heating

With diborane; trichlorophosphate; In tetrahydrofuran;