N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine

Base Information

Chemical Name:N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine
CAS No.:117125-42-5
Molecular Formula:C₁₆H₁₅NO₂S
Molecular Weight:285.367
Hs Code.:
DSSTox Substance ID:DTXSID40922297
ChEMBL ID:CHEMBL1733540

Synonyms:BRN 4492799;N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine;Glycine, N-(6,11-dihydrodibenzo(b,e)thiepin-11-yl)-;117125-42-5;2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetic acid;N-(6,11-Dihydrodibenzo[b,e]thiepin-11-yl)glycine;MLS001179376;CHEMBL1733540;DTXSID40922297;HMS2781B10;LS-72496;SMR000475884;(6,11-dihydrodibenzo[b,e]thiepin-11-ylamino)acetic acid

Suppliers and Price of N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine

Chemical Property:

Vapor Pressure:7.4E-10mmHg at 25°C
Boiling Point:475.7°C at 760 mmHg
Flash Point:241.5°C
Density:1.33g/cm³
XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:285.08234989
Heavy Atom Count:20
Complexity:349

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C(C3=CC=CC=C3S1)NCC(=O)O

Technology Process of N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine

There total 2 articles about N-(6,11-Dihydrodibenzo(b,e)thiepin-11-yl)glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 117125-39-0
ethyl 2-(6,11-dihydrodibenzothiepin-11-ylamino)acetate

: 117125-42-5
2-(6,11-dihydrodibenzothiepin-11-ylamino)acetic acid

Guidance literature:: With sodium hydroxide; water; acetic acid; In methanol; for 1.5h; Heating;

Reference yield:

: 1745-53-5
11-amino-6,11-dihydrodibenzothiepin

: 117125-42-5
2-(6,11-dihydrodibenzothiepin-11-ylamino)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / toluene / 32 h / Heating

2: 60 percent / 1) 10percent NaOH, H₂O; 2) 2.5M-CH₃COOH / methanol / 1.5 h / Heating

With sodium hydroxide; water; potassium carbonate; acetic acid; In methanol; toluene;