[1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene

Base Information

Chemical Name:[1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene
CAS No.:23538-45-6
Molecular Formula:C₁₅H₂₂O
Molecular Weight:218.339
Hs Code.:
Mol file:23538-45-6.mol

Synonyms:2-Propen-1-one,1-(2,3,5,6,7,7a-hexahydro-7,7a-dimethyl-1H-inden-1-yl)-2-methyl-, [1R-(1a,7b,7ab)]-; Chiloscyphone

Suppliers and Price of [1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene

Chemical Property:

PSA：17.07000
LogP:3.90420

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene

There total 72 articles about [1R,(-)]-1α-(2-Methylenepropanoyl)-7β,7aβ-dimethyl-2,3,5,6,7,7a-hexahydro-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 13291-18-4
isopropenylmagnesium bromide

: 122689-44-5,125639-06-7,130794-46-6
<(5R*,6R*,7R*)-5,6-Dimethylbicyclo<4.3.0>non-1-en-7-yl>methanol

: 23538-45-6,97806-72-9,130605-61-7
(+/-)-chiloscyphone

Guidance literature:: <(5R*,6R*,7R*)-5,6-Dimethylbicyclo<4.3.0>non-1-en-7-yl>methanol; With dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; at 20 ℃; for 1h;

isopropenylmagnesium bromide; In tetrahydrofuran; at 0 ℃; for 0.5h;

With dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200500928