1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]-

Base Information

Chemical Name:1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]-
CAS No.:62893-27-0
Molecular Formula:C24H14BrClN4O3
Molecular Weight:521.757
Hs Code.:

Synonyms:5-chloro-2-[3-bromo-5-(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]benzophenone;2-[4-(2-Benzoyl-4-chloro-phenyl)-5-bromo-4H-[1,2,4]triazol-3-ylmethyl]-isoindole-1,3-dione;

Suppliers and Price of 1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]-

Chemical Property:

PSA：85.16000
LogP:4.64830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]-

There total 5 articles about 1H-Isoindole-1,3(2H)-dione, 2-[[4-(2-benzoyl-4-chlorophenyl)-5-bromo-4H-1,2,4-triazol-3-yl]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.6%

: 54485-85-7
N-[4-(2-benzoyl-4-chloro-phenyl)-4H-[1,2,4]triazol-3-ylmethyl]-phthalimide

: 62893-27-0
N-[4-(2-benzoyl-4-chloro-phenyl)-5-bromo-4H-[1,2,4]triazol-3-ylmethyl]-phthalimide

Guidance literature:: With N-Bromosuccinimide; In benzene; for 7h; Heating;
DOI:10.1002/jhet.5570170331

Reference yield:

: 59010-35-4
1,3-Dioxo-2-isoindolineacetic Acid, <methylene>hydrazine

: 62893-27-0
N-[4-(2-benzoyl-4-chloro-phenyl)-5-bromo-4H-[1,2,4]triazol-3-ylmethyl]-phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / trifluoroacetic acid / toluene / 1.5 h / 100 - 110 °C

2: 77.6 percent / N-bromosuccinimide / benzene / 7 h / Heating

With N-Bromosuccinimide; trifluoroacetic acid; In toluene; benzene;
DOI:10.1002/jhet.5570170331

Reference yield:

: 6780-38-7
N-phthaloylglycine chloride

: 62893-27-0
N-[4-(2-benzoyl-4-chloro-phenyl)-5-bromo-4H-[1,2,4]triazol-3-ylmethyl]-phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 90.7 percent / pyridine / tetrahydrofuran / 6 h / 0 - 25 °C

2: 53 percent / trifluoroacetic acid / toluene / 1.5 h / 100 - 110 °C

3: 77.6 percent / N-bromosuccinimide / benzene / 7 h / Heating

With pyridine; N-Bromosuccinimide; trifluoroacetic acid; In tetrahydrofuran; toluene; benzene;
DOI:10.1002/jhet.5570170331