6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione
CAS No.:62925-51-3
Molecular Formula:C₁₂H₁₃N₃O₂S
Molecular Weight:263.32
Hs Code.:
DSSTox Substance ID:DTXSID70490419
Wikidata:Q82334181

Synonyms:62925-51-3;DTXSID70490419;6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione

Suppliers and Price of 6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:263.07284784
Heavy Atom Count:18
Complexity:397

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=CC(=O)N(C1=O)C)SC2=CC=CC=C2N

Technology Process of 6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione

There total 1 articles about 6-[(2-Aminophenyl)sulfanyl]-1,3-dimethylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62925-51-3
1,3-dimethyl-6-(2-aminophenylthio)uracil

Guidance literature:: /BRN= 144393/, 2-Thio-anilin, Triethylamin;
DOI:10.1055/s-1977-24310

Reference yield: 40.0%

: 64-19-7,77671-22-8
acetic acid

: 62925-51-3
1,3-dimethyl-6-(2-aminophenylthio)uracil

: 74502-69-5
1,3-dimethyl-6-(2-acetamidophenylthio)uracil

: 76965-85-0
1,3-bis((2-benzothiazolyl)acetyl)-1,3-dimethylurea

Guidance literature:: for 4h; Mechanism; Heating; further derivatives, further reactant;
DOI:10.1016/0040-4020(80)80097-4

Reference yield:

: 62925-51-3
1,3-dimethyl-6-(2-aminophenylthio)uracil

: 76965-83-8
1,3-dimethyl-5-acetyl-6-(2-methylthioanilino)uracil

Guidance literature:: Multi-step reaction with 4 steps

1: 1 g / pyridine / Ambient temperature

2: 0.6 g / NaOH / methanol; H₂O

3: alkali / methanol / Ambient temperature

4: pyridine / Ambient temperature

With pyridine; sodium hydroxide; In methanol; water;
DOI:10.1016/0040-4020(80)80097-4