N-(3,5-Dimethylphenyl)-N-methylnitrous amide

Base Information

Chemical Name:N-(3,5-Dimethylphenyl)-N-methylnitrous amide
CAS No.:62959-13-1
Molecular Formula:C9H12N2O
Molecular Weight:164.207
Hs Code.:
DSSTox Substance ID:DTXSID70513410
Wikidata:Q82373213

Synonyms:N-(3,5-Dimethylphenyl)-N-methylnitrous amide;62959-13-1;DTXSID70513410

Suppliers and Price of N-(3,5-Dimethylphenyl)-N-methylnitrous amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,5-Dimethylphenyl)-N-methylnitrous amide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:164.094963011
Heavy Atom Count:12
Complexity:151

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)N(C)N=O)C

Technology Process of N-(3,5-Dimethylphenyl)-N-methylnitrous amide

There total 4 articles about N-(3,5-Dimethylphenyl)-N-methylnitrous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13342-20-6
N-methyl-3,5-dimethylaniline

: 62959-13-1
N-nitroso-N,3,5-trimethylaniline

Guidance literature:: With sulfuric acid; sodium nitrite; In water; at 10 ℃;
DOI:10.1021/jo00348a016

Reference yield:

: 114097-28-8
N-(3,5-dimethylphenyl)-4-methyl-benzenesulfonamide

: 62959-13-1
N-nitroso-N,3,5-trimethylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 5percent NaOH / H₂O / 40 - 70 °C

2: 80percent H₂SO₄ / 0.33 h / 160 °C

3: 93 percent / NaNO₂, 25percent H₂SO₄ / H₂O / 10 °C

With sodium hydroxide; sulfuric acid; sodium nitrite; In water;
DOI:10.1021/jo00348a016

Reference yield:

: 80387-74-2
N-methyl-N-(3,5-dimethylphenyl)-4-toluenesulfonamide

: 62959-13-1
N-nitroso-N,3,5-trimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 80percent H₂SO₄ / 0.33 h / 160 °C

2: 93 percent / NaNO₂, 25percent H₂SO₄ / H₂O / 10 °C

With sulfuric acid; sodium nitrite; In water;
DOI:10.1021/jo00348a016