4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide
CAS No.:73774-60-4
Molecular Formula:C17H18N2O2S
Molecular Weight:314.402
Hs Code.:
NSC Number:314073
DSSTox Substance ID:DTXSID50429742

Synonyms:NSC314073;73774-60-4;DTXSID50429742;NSC-314073

Suppliers and Price of 4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide

Chemical Property:

Boiling Point:471.8°Cat760mmHg
Flash Point:239.1°C
Density:1.13g/cm³
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:314.10889899
Heavy Atom Count:22
Complexity:473

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NN=CC2=CC=CC=C2CC=C
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)N/N=C/C2=CC=CC=C2CC=C

Technology Process of 4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide

There total 1 articles about 4-methyl-N-[(E)-(2-prop-2-enylphenyl)methylideneamino]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 62708-42-3
o-allylbenzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 73774-60-4
o-Allylbenzaldehyde Tosylhydrazone

Guidance literature:: In methanol; at 40 ℃; for 0.5h;
DOI:10.1021/jo01307a008

Reference yield:

: 73774-60-4
o-Allylbenzaldehyde Tosylhydrazone

: 73774-59-1
4,5-Dihydro-1,4-methano-1H-2,3-benzodiazepine

: 73774-56-8
2,3,4,5-Tetrahydro-3-<(4-methylphenyl)sulfonyl>-1,4-methano-1H-2,3-benzodiazepine

Guidance literature:: With boron trifluoride diethyl etherate; In benzene; for 6h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo01307a008

Reference yield:

: 73774-60-4
o-Allylbenzaldehyde Tosylhydrazone

: 15677-15-3,148323-54-0,148323-57-3
benzo[2,3]bicyclo[3.1.0]hexane

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃ etherate / benzene / 6 h / Ambient temperature

2: 98 percent / benzene / 5 h / 130 °C / sealed tube

With boron trifluoride diethyl etherate; In benzene;
DOI:10.1021/jo01307a008