Benzene, 1-bromo-2-(2-iodoethyl)-3-methoxy-5-methyl-

Base Information

Chemical Name:Benzene, 1-bromo-2-(2-iodoethyl)-3-methoxy-5-methyl-
CAS No.:630120-27-3
Molecular Formula:C10H12BrIO
Molecular Weight:355.013
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 1-bromo-2-(2-iodoethyl)-3-methoxy-5-methyl-

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Technology Process of Benzene, 1-bromo-2-(2-iodoethyl)-3-methoxy-5-methyl-

There total 6 articles about Benzene, 1-bromo-2-(2-iodoethyl)-3-methoxy-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 630120-22-8
2-(2-bromo-6-methoxy-4-methylphenyl)ethanol

: 630120-27-3
1-bromo-2-(2-iodoethyl)-3-methoxy-5-methylbenzene

Guidance literature:: 2-(2-bromo-6-methoxy-4-methylphenyl)ethanol; With methanesulfonyl chloride; triethylamine; In dichloromethane; for 2h;

With sodium iodide; In acetone; for 24h; Heating;

Reference yield:

: 133129-29-0
2-bromo-6-methoxy-4-methylbenzaldehyde

: 630120-27-3
1-bromo-2-(2-iodoethyl)-3-methoxy-5-methylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: (Me₃Si)2NK / toluene / 1 h

1.2: 76 percent / toluene / 10 h

2.1: 9-BBN / tetrahydrofuran / 10 h / 0 - 20 °C

2.2: 87 percent / aq. NaOH; aq. H₂O₂ / methanol / 2 h

3.1: Et₃N; MsCl / CH₂Cl₂ / 2 h

3.2: 92 percent / NaI / acetone / 24 h / Heating

With 9-borabicyclo[3.3.1]nonane dimer; potassium hexamethylsilazane; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 1.2: Wittig reaction;

Reference yield:

: 630120-19-3
2-bromo-6-methoxy-4-methylphenylacetaldehyde

: 630120-27-3
1-bromo-2-(2-iodoethyl)-3-methoxy-5-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / DIBAL-H / cyclohexane; CH₂Cl₂ / 0.5 h

2.1: Et₃N; MsCl / CH₂Cl₂ / 2 h

2.2: 92 percent / NaI / acetone / 24 h / Heating

With diisobutylaluminium hydride; methanesulfonyl chloride; triethylamine; In dichloromethane; cyclohexane;