N-(2-Chloroethyl)cinnamamide

Base Information Edit

Chemical Name:N-(2-Chloroethyl)cinnamamide
CAS No.:30687-03-7
Molecular Formula:C11H12 Cl N O
Molecular Weight:209.675
Hs Code.:2924299090
Nikkaji Number:J48.412A
Wikidata:Q76325771
Mol file:30687-03-7.mol

Synonyms:N-(2-Chloroethyl)cinnamamide;BRN 2328045;CINNAMAMIDE, N-(2-CHLOROETHYL)-;30687-03-7;2-Propenamide, N-(2-chloroethyl)-3-phenyl-;N-(2-Chloroethyl)-3-phenylpropenamide;LS-53888

Suppliers and Price of N-(2-Chloroethyl)cinnamamide

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(2-Chloroethyl)cinnamamide Edit

Chemical Property:

Vapor Pressure:6.84E-07mmHg at 25°C
Boiling Point:408.8°Cat760mmHg
Flash Point:201°C
PSA：32.59000
Density:1.16g/cm³
LogP:2.89510
XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:209.0607417
Heavy Atom Count:14
Complexity:198

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC(=O)NCCCl
Isomeric SMILES:C1=CC=C(C=C1)/C=C/C(=O)NCCCl

Technology Process of N-(2-Chloroethyl)cinnamamide

There total 5 articles about N-(2-Chloroethyl)cinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 870-24-6
2-chloroethanamine hydrochloride

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 30687-03-7
(E)-N-(2-chloroethyl)cinnamamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 621-82-9
Cinnamic acid

: 30687-03-7
(Z)-N-(2-Chloro-ethyl)-3-phenyl-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 24 h / Reflux

2: potassium hydroxide / chloroform; water / 3.5 h / Cooling with ice

With thionyl chloride; potassium hydroxide; In chloroform; water; 2: |Schotten-Baumann Reaction;
DOI:10.2478/s11696-013-0405-x