4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine

Base Information

• Chemical Name: 4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine
• CAS No.: 3025-42-1
• Molecular Formula: C16H17 Cl N4 O2
• Molecular Weight: 332.79
• DSSTox Substance ID: DTXSID001031234
• Nikkaji Number: J428.471B
• Mol file: 3025-42-1.mol

Synonyms:CCRIS 7409;4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine;3025-42-1;SCHEMBL7178174;SCHEMBL11955370;4-[(2-chloro-4-nitrophenyl)diazenyl]-N,N-diethylaniline;DTXSID001031234;LS-188295;2-Chloro-4'-(diethylamino)-4-nitroazobenzene

Chemical Property of 4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine

Chemical Property:

• Vapor Pressure: 5.74E-10mmHg at 25°C
• Boiling Point: 495.8°Cat760mmHg
• Flash Point: 253.6°C
• PSA: 73.78000
• Density: 1.24g/cm³
• LogP: 6.03300
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 332.1040035
• Heavy Atom Count: 23
• Complexity: 403

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC=C(C=C1)N=NC2=C(C=C(C=C2)[N+](=O)[O-])Cl

Technology Process of 4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine

There total 1 articles about 4-((2-Chloro-4-nitrophenyl)azo)-N,N-diethylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloro-4-nitroaniline (121-87-9) + N,N-diethylaniline (91-66-7) → p-<(2'-Chlor-4'-nitrophenyl)-azo>-(N,N,-diethyl)-anilin (3025-42-1)

Guidance literature:

With hydrogenchloride; sodium acetate; sodium nitrite; Multistep reaction; 1.) H₂O, 0-8 deg C, 1 h, 2.) aq. CH₃COOH, 2 h, 0-5 deg C;

upstream raw materials:

2-Chloro-4-nitroaniline

N,N-diethylaniline

Refernces

• 1、 Haessner, Carmen,Mustroph, H.. "Studies on UV/Vis Absorption Spectra of Azo Dyes. XVIII. Substituent Effects on the Absorption Maxima of the n-->?* and ?-->?* Bands of 4-N,N-Diethylaminoazobenzenes". . p. 493 - 498. Retrieved 2007/10/02.