Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]-

Base Information

Chemical Name:Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]-
CAS No.:63072-15-1
Molecular Formula:C27H20NOP
Molecular Weight:405.436
Hs Code.:

Synonyms:Benzonitrile,4-[(triphenylphosphoranylidene)acetyl];4-[(Triphenylphosphoranylidene)acetyl]benzonitrile;4-[2-(triphenylphosphosphanylidene)acetyl]benzonitrile;4-[2-(triphenyl;Triphenylphosphine-P-cyanobenzoylmethylene;4-[2-(triphenylphosphanylidene)acetyl]benzonitrile;

Suppliers and Price of Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]-

Chemical Property:

Boiling Point:612.0±57.0 °C(Predicted)
PSA：50.67000
Density:1.22±0.1 g/cm3(Predicted)
LogP:4.53728

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]-

There total 5 articles about Benzonitrile, 4-[(triphenylphosphoranylidene)acetyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 20099-89-2
4-Cyanophenacyl bromide

: 603-35-0
triphenylphosphine

: 63072-15-1
4-[2-(triphenylphosphosphanylidene)acetyl]benzonitrile

Guidance literature:: 4-Cyanophenacyl bromide; triphenylphosphine; In acetone; at 40 ℃; for 12h;

With sodium hydroxide; In water;
DOI:10.1002/aoc.5265

Reference yield:

: 374671-36-0
Br^(1-)*C₂₇H₂₁NOP⁽¹⁺⁾

: 63072-15-1
4-[2-(triphenylphosphosphanylidene)acetyl]benzonitrile

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃; for 1h;
DOI:10.1021/ol901758k

Reference yield:

: 603-35-0
triphenylphosphine

: 63072-15-1
4-[2-(triphenylphosphosphanylidene)acetyl]benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 3 h / 20 °C

2: potassium carbonate / acetonitrile / 3 h

With potassium carbonate; In acetonitrile;
DOI:10.1002/chem.201602992