Cyclobutanol, 2-[1-methyl-2-(phenylthio)ethyl]-1-[1-(phenylthio)cyclopropyl]-

Base Information

Chemical Name:Cyclobutanol, 2-[1-methyl-2-(phenylthio)ethyl]-1-[1-(phenylthio)cyclopropyl]-
CAS No.:63073-05-2
Molecular Formula:C22H26OS2
Molecular Weight:370.58
Hs Code.:

Synonyms:

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Chemical Property of Cyclobutanol, 2-[1-methyl-2-(phenylthio)ethyl]-1-[1-(phenylthio)cyclopropyl]-

Chemical Property:

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Technology Process of Cyclobutanol, 2-[1-methyl-2-(phenylthio)ethyl]-1-[1-(phenylthio)cyclopropyl]-

There total 2 articles about Cyclobutanol, 2-[1-methyl-2-(phenylthio)ethyl]-1-[1-(phenylthio)cyclopropyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14633-54-6
cyclopropylphenylsulfide

: 63073-05-2
1-(1'-Phenylthiocycloprop-1'-yl)-2-(1'-phenylthioprop-2'-yl)-cyclobutan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: (i) nBuLi, THF, (ii) /BRN= 1817781/, (iii) TsOH, benzene

2: (i) nBuLi, (ii) /BRN= 2503992/

DOI:10.1021/ja00451a040

Reference yield:

: 14633-54-6
cyclopropylphenylsulfide

: 56102-07-9
2-(1-Methyl-2-phenylsulfanyl-ethyl)-cyclobutanone

: 63073-05-2
1-(1'-Phenylthiocycloprop-1'-yl)-2-(1'-phenylthioprop-2'-yl)-cyclobutan-1-ol

Guidance literature:: Multistep reaction; (i) nBuLi, (ii) /BRN= 2503992/;
DOI:10.1021/ja00451a040

Reference yield:

: 63073-05-2
1-(1'-Phenylthiocycloprop-1'-yl)-2-(1'-phenylthioprop-2'-yl)-cyclobutan-1-ol

: 26532-22-9,28117-21-7,30346-21-5,30820-22-5,51937-29-2,54088-78-7,68225-45-6,108645-56-3
grandisol

Guidance literature:: Multi-step reaction with 10 steps

1: TsOH / benzene

2: pyridinium bromide perbromide / acetic acid

3: AgNO₃

4: LiAlH₄ / tetrahydrofuran

5: Et₃N, Py*SO₃ / dimethylsulfoxide

6: KOH, N₂H₄*H₂O, triethylene glycol

7: aq. HCl / tetrahydrofuran

8: LiAlH₄ / diethyl ether

9: MCPBA / CH₂Cl₂

10: CaCO₃ / decahydronaphthalene

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; pyridinium hydrobromide perbromide; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; hydrazine hydrate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; dimethyl sulfoxide; decalin; benzene;
DOI:10.1021/ja00451a040