6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone

Base Information

Chemical Name:6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone
CAS No.:58186-01-9
Molecular Formula:C13H16O6
Molecular Weight:268.266
Hs Code.:
Mol file:58186-01-9.mol

Synonyms:6-(3-carboxypropyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone;QS-4;6-(-carboxypropyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone;2,3-Dimethoxy-5-methyl-6-(3-carboxypropyl)-1,4-benzochinon;

Suppliers and Price of 6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
QS-4-D6 95.00%
5MG
$ 502.57

Total 14 raw suppliers

Chemical Property of 6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone

Chemical Property:

Melting Point:74-75 °C(Solv: hexane (110-54-3); ethyl ether (60-29-7))
Boiling Point:494.3±45.0 °C(Predicted)
PKA:4.65±0.10(Predicted)
PSA：89.90000
Density:1.26±0.1 g/cm3(Predicted)
LogP:1.21400

Purity/Quality:

99% ^*data from raw suppliers

QS-4-D6 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone

There total 5 articles about 6-(3-carboxypropyl)-2,3-diMethoxy-5-Methyl-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 58185-87-8
4-(2'-hydroxy-3',4'-dimethoxy-6'-methylphenyl)butyric acid

: 58186-01-9
2,3-dimethoxy-5-methyl-6-(3'-carboxypropyl)-1,4-benzoquinone

Guidance literature:: With sodium hydroxide; potassium nitrososulfonate; In water; for 1h; Ambient temperature;
DOI:10.1248/cpb.30.2797

Reference yield: 25.0%

: 110-94-1
1,5-pentanedioic acid

: 605-94-7
2,3-Dimethoxy-5-methyl-1,4-benzoquinone

: 58186-01-9
2,3-dimethoxy-5-methyl-6-(3'-carboxypropyl)-1,4-benzoquinone

Guidance literature:: With ammonium peroxydisulfate; silver nitrate; In water; acetonitrile; at 75 ℃; for 1h;
DOI:10.3390/molecules26051382

Reference yield:

: 6443-69-2
3,4,5-trimethoxytoluene

: 58186-01-9
2,3-dimethoxy-5-methyl-6-(3'-carboxypropyl)-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) AlCl₃, 2.) 12percent methanolic KOH / 1.) nitrobenzene, 0 deg C, 6 h, RT, 64 h

2: 67 percent / Zn/Hg, conc. HCl / toluene / 15 h / Heating

3: 82 percent / ON(SO₃K)2, 1percent NaOH / H₂O / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium hydroxide; aluminium trichloride; potassium nitrososulfonate; mercury; zinc; In water; toluene;
DOI:10.1248/cpb.30.2797