Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, hydrochloride, hydrate(2:2:1)

Base Information

• Chemical Name: Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, hydrochloride, hydrate(2:2:1)
• CAS No.: 218282-71-4
• Molecular Formula: C₁₇H₂₇Cl₂N₅*ClH*0H₂O
• Molecular Weight: 417.809
• Mol file: 218282-71-4.mol

Synonyms:Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, monohydrochloride, hydrate(2:1) (9CI); Olanexidine hydrochloride hydrate

Chemical Property of Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, hydrochloride, hydrate(2:2:1)

Chemical Property:

• Boiling Point: 503.3oC at 760 mmHg
• Flash Point: 258.2oC
• PSA: 176.81000
• LogP: 13.26850

Purity/Quality:

98% ^*data from raw suppliers

OlanexidineHydrochloridesemihydrate;OPB-2045,OPB-2045G >98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, hydrochloride, hydrate(2:2:1)

There total 3 articles about Imidodicarbonimidicdiamide, N-[(3,4-dichlorophenyl)methyl]-N'-octyl-, hydrochloride, hydrate(2:2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.4%

1-(3,4-dichlorobenzyl)-5-octylbiguanide dihydrochloride → 1-(3,4-dichlorobenzyl)-5-octylbiguanide monohydrochloride semihydrate (218282-71-4)

Guidance literature:

With ethanol; water; at 10 - 40 ℃; for 2h; Product distribution / selectivity; Heating / reflux;

Reference yield: 96.5%

→ 1-(3,4-dichlorobenzyl)-5-octylbiguanide monohydrochloride semihydrate (218282-71-4)

Guidance literature:

In ethanol; water; at 10 - 80 ℃; for 1.5h; Purification / work up;

Reference yield: 77.2%

N-octyl-N'-cyanoguanidine (60852-95-1) + 3,4-dichlorobenzyl amine (102-49-8) → 1-(3,4-dichlorobenzyl)-5-octylbiguanide monohydrochloride semihydrate (218282-71-4)

Guidance literature:

N-octyl-N'-cyanoguanidine; 3,4-dichlorobenzyl amine; With hydrogenchloride; In acetic acid butyl ester; water; at 35 ℃; for 6.5h; Heating / reflux;

With hydrogenchloride; In acetic acid butyl ester; water; isopropyl alcohol; at 10 - 80 ℃; for 1h; Product distribution / selectivity;

upstream raw materials:

N-octyl-N'-cyanoguanidine

3,4-dichlorobenzyl amine

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