3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine

Base Information

Chemical Name:3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine
CAS No.:63119-34-6
Molecular Formula:C18H17N3O3
Molecular Weight:323.351
Hs Code.:
DSSTox Substance ID:DTXSID60506538
Wikidata:Q82362325

Synonyms:3-methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine;63119-34-6;SCHEMBL11237449;DTXSID60506538;RDQUCZOJBAGKNW-UHFFFAOYSA-N;3-methoxy-5,6-bis-(4-methoxyphenyl)-1,2,4-triazine

Suppliers and Price of 3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:323.12699141
Heavy Atom Count:24
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=C(N=NC(=N2)OC)C3=CC=C(C=C3)OC

Technology Process of 3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine

There total 4 articles about 3-Methoxy-5,6-bis(4-methoxyphenyl)-1,2,4-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 58848-77-4
3-methylthio-5,6-bis(4-methoxyphenyl)-1,2,4-triazine

: 63119-34-6
5,6-bis(4-methoxyphenyl)-3-methoxy-1,2,4-triazine

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;
DOI:10.1021/jo01311a007

Reference yield:

: 59663-39-7
3-chloro-5,6-bis-(4-methoxy-phenyl)-[1,2,4]triazine

: 63119-34-6
5,6-bis(4-methoxyphenyl)-3-methoxy-1,2,4-triazine

Guidance literature:: In methanol;

Reference yield:

: 1226-42-2
1,2-bis(4-methoxyphenyl)-1,2-ethanedione

: 63119-34-6
5,6-bis(4-methoxyphenyl)-3-methoxy-1,2,4-triazine

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / sodium bicarbonate / methanol / 8 h / 60 °C

2: 91 percent / sodium borohydride / tetrahydrofuran; methanol / 23 h / Ambient temperature

3: 1) sodium hydride / 1) DMF, 15 min; 2) room temp., 3 h

4: 60 percent / toluene / 12 h / 110 °C

With sodium tetrahydroborate; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/jo01311a007