Triethyl(1-phenylethenyl)germane

Base Information

Chemical Name:Triethyl(1-phenylethenyl)germane
CAS No.:63139-22-0
Molecular Formula:C14H22Ge
Molecular Weight:262.919
Hs Code.:
DSSTox Substance ID:DTXSID70537116
Nikkaji Number:J1.124.523D
Wikidata:Q82411992

Synonyms:Triethyl(1-phenylethenyl)germane;63139-22-0;DTXSID70537116

Suppliers and Price of Triethyl(1-phenylethenyl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Triethyl(1-phenylethenyl)germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:264.0933285
Heavy Atom Count:15
Complexity:189

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Ge](CC)(CC)C(=C)C1=CC=CC=C1

Technology Process of Triethyl(1-phenylethenyl)germane

There total 3 articles about Triethyl(1-phenylethenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1188-14-3
Triethylgerman

: 536-74-3
phenylacetylene

: 63139-22-0
1-(triethylgermyl)-1-phenylethene

: 19319-12-1
trans-1-phenyl-2-(triethylgermyl)ethene

Guidance literature:: Rh(acac)(cyclooctene)(PCy₃); In benzene-d6; Ar-atmosphere; 48 h at room temp.;
DOI:10.1021/om981042n

Reference yield: 74.0%

: 325747-42-0
(Z)-1-(tributylstannyl)-2-(triethylgermyl)-1-phenylethene

: 63139-22-0
1-(triethylgermyl)-1-phenylethene

: 19319-12-1
trans-1-phenyl-2-(triethylgermyl)ethene

Guidance literature:: With hydrogen iodide; tetra-(n-butyl)ammonium iodide; In toluene; reagents mixed and stirred at 0°C for 1 h, washed with aqueous NaHCO3, organic layer treated with aqueous KF; purified by column chromy.;
DOI:10.1246/cl.2000.1408