1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine

Base Information

Chemical Name:1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine
CAS No.:84646-82-2
Molecular Formula:C₂₁H₂₄N₂O₃
Molecular Weight:352.433
Hs Code.:
DSSTox Substance ID:DTXSID301004939
Mol file:84646-82-2.mol

Synonyms:2-(4-Methylpiperazinomethyl)dibenz(2,3:6,7)-3a,12b-dihydrooxepin(4,5-d)-1,3-dioxolane;84646-82-2;1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine;Piperazine, 1-((3a,12b-dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methyl-;DTXSID301004939;LS-111572;1-[(3a,12b-Dihydro-2H-dibenzo[b,f][1,3]dioxolo[4,5-d]oxepin-2-yl)methyl]-4-methylpiperazine

Suppliers and Price of 1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PIPERAZINE, 1-((3A,12B-DIHYDRODIBENZO(B,F)-1,3-DIOXOLO(4,5-D)OXEPIN-2-YL)METHYL)-4-METHYL- 95.00%
5MG
$ 500.81

Total 0 raw suppliers

Chemical Property of 1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine

Chemical Property:

Vapor Pressure:1.62E-08mmHg at 25°C
Boiling Point:456.4°C at 760 mmHg
Flash Point:130.4°C
PSA：34.17000
Density:1.201g/cm³
LogP:3.07080
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:352.17869263
Heavy Atom Count:26
Complexity:452

Purity/Quality:: PIPERAZINE, 1-((3A,12B-DIHYDRODIBENZO(B,F)-1,3-DIOXOLO(4,5-D)OXEPIN-2-YL)METHYL)-4-METHYL- 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCN(CC1)CC2OC3C(O2)C4=CC=CC=C4OC5=CC=CC=C35

Technology Process of 1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine

There total 3 articles about 1-((3a,12b-Dihydrodibenzo(b,f)-1,3-dioxolo(4,5-d)oxepin-2-yl)methyl)-4-methylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 109-01-3
1-methyl-piperazine

: 84646-76-4
2-(2-Chloroethyl)dibenz<2,3:6,7>-3a,12b-dihydrooxepin<4,5-d>-1,3-dioxolane

: 84646-82-2
2-(4-methyl-piperazinomethyl)dibenz<2,3:6,7>-3a,12b-dihydrooxepin<4,5-d>-1,3-dioxolane

Guidance literature:: In toluene; for 20h; Heating;

Reference yield:

: 13691-53-7
10,11-dibromo-10,11-dihydrodibenzoxepine

: 84646-82-2
2-(4-methyl-piperazinomethyl)dibenz<2,3:6,7>-3a,12b-dihydrooxepin<4,5-d>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) AcOAg; 2.) KOH / 1.) H₂O, AcOH, 80 deg C, 5 h; 2.) MeOH, refl., 10 min

2: 0.25 g / 0.17 h / 105 °C

3: 76 percent / toluene / 20 h / Heating

With potassium hydroxide; silver(I) acetate; In toluene;

Reference yield:

: 77368-83-3
Cis-10,11-dihydroxy-10,11-dihydrodibenzoxepine

: 84646-82-2
2-(4-methyl-piperazinomethyl)dibenz<2,3:6,7>-3a,12b-dihydrooxepin<4,5-d>-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 0.25 g / 0.17 h / 105 °C

2: 76 percent / toluene / 20 h / Heating

In toluene;