L-Phenylalanine, N-formyl-4-(1H-pyrazol-1-yl)-

Base Information

Chemical Name:L-Phenylalanine, N-formyl-4-(1H-pyrazol-1-yl)-
CAS No.:632297-66-6
Molecular Formula:C13H13N3O3
Molecular Weight:259.265
Hs Code.:

Synonyms:

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Chemical Property of L-Phenylalanine, N-formyl-4-(1H-pyrazol-1-yl)-

Chemical Property:

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Technology Process of L-Phenylalanine, N-formyl-4-(1H-pyrazol-1-yl)-

There total 4 articles about L-Phenylalanine, N-formyl-4-(1H-pyrazol-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-formyl-4-iodo-L-phenylalanine methyl ester

: 632297-66-6
N-formyl-4-(1H-pyrazol-1-yl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / methanol; water / 4 h / 22 °C

1.2: 1 - 2 h / 31 °C / pH 1

2.1: copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium carbonate / 1-methyl-pyrrolidin-2-one / 15 h / 125 °C

With sodium hydroxide; copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium carbonate; In 1-methyl-pyrrolidin-2-one; methanol; water;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 632297-66-6
N-formyl-4-(1H-pyrazol-1-yl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 3 steps

1.1: peracetic acid; sulfuric acid; iodine; acetic acid / 2 - 4 h / 55 °C

1.2: 2 h / 50 - 55 °C

1.3: 1 h / 10 - 15 °C

2.1: sodium hydroxide / methanol; water / 4 h / 22 °C

2.2: 1 - 2 h / 31 °C / pH 1

3.1: copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium carbonate / 1-methyl-pyrrolidin-2-one / 15 h / 125 °C

With peracetic acid; sodium hydroxide; copper(l) iodide; sulfuric acid; trans-1,2-Diaminocyclohexane; iodine; potassium carbonate; acetic acid; In 1-methyl-pyrrolidin-2-one; methanol; water;

Reference yield:

: 1991-81-7,14173-41-2,24250-85-9,62561-75-5
4-iodo-L-phenylalanine

: 632297-66-6
N-formyl-4-(1H-pyrazol-1-yl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / 3 h / 50 - 60 °C

2.1: acetic anhydride / toluene / 2 h / 10 - 15 °C

3.1: sodium hydroxide / methanol; water / 4 h / 19 - 25 °C

3.2: 1.83 - 3 h / -3 - 33 °C / pH 1

4.1: (±)-1,2-trans.-cyclohexanediamine; copper(l) iodide; potassium carbonate / 1-methyl-pyrrolidin-2-one / 15 h / 20 - 128 °C

4.2: 1.17 h / 0 - 6 °C / pH 1

With (±)-1,2-trans.-cyclohexanediamine; sodium hydroxide; copper(l) iodide; thionyl chloride; acetic anhydride; potassium carbonate; In 1-methyl-pyrrolidin-2-one; methanol; water; toluene;