2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI)

Base Information

Chemical Name:2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI)
CAS No.:632335-63-8
Molecular Formula:C6H9NS
Molecular Weight:127.20700
Hs Code.:
Mol file:632335-63-8.mol

Synonyms:1-Methyl-5,6-dihydro-1H-pyridine-2-thione;1-methyl-5,6-dihydropyridine-2(1H)-thione;

Suppliers and Price of 2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI)

Chemical Property:

Melting Point:76 - 77 °C
PSA：35.33000
LogP:1.14340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI)

There total 2 articles about 2(1H)-Pyridinethione,5,6-dihydro-1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1111141-19-5
1-methyl-3,6-dihydro-1H-pyridine-2-thione

: 632335-63-8
1-methyl-5,6-dihydro-1H-pyridine-2-thione

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.10.113

Reference yield: 50.0%

: 13070-07-0
1-methylpiperidine-2-thione

: 632335-63-8
1-methyl-5,6-dihydro-1H-pyridine-2-thione

Guidance literature:: 1-methylpiperidine-2-thione; With methyl benzenesulfinate; sodium hydride; In tetrahydrofuran; for 1h; Heating;

With sodium carbonate; In toluene; for 1h; Heating;
DOI:10.1055/s-2003-41016

Reference yield: 96.0%

: 1122-60-7
1-nitrocyclohexane

: 632335-63-8
1-methyl-5,6-dihydro-1H-pyridine-2-thione

: 1127344-25-5
1-methyl-4-(1-nitrocyclohexyl)piperidine-2-thione

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 4h; regioselective reaction;
DOI:10.1016/j.tet.2008.12.037