3-(5-Chloro-2-methoxyphenyl)prop-2-enal

Base Information

Chemical Name:3-(5-Chloro-2-methoxyphenyl)prop-2-enal
CAS No.:33538-90-8
Molecular Formula:C10H9ClO2
Molecular Weight:196.6303
Hs Code.:
NSC Number:110722
DSSTox Substance ID:DTXSID00419037
Wikidata:Q82229824

Synonyms:NSC110722;33538-90-8;DTXSID00419037;NSC-110722;3-(5-chloro-2-methoxyphenyl)prop-2-enal;CS-0302896;(E)-3-(5-Chloro-2-methoxyphenyl)acrylaldehyde;EN300-1963575;1204348-46-8

Suppliers and Price of 3-(5-Chloro-2-methoxyphenyl)prop-2-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-(5-Chloro-2-methoxyphenyl)prop-2-enal

Chemical Property:

Vapor Pressure:0.000151mmHg at 25°C
Boiling Point:331.9°Cat760mmHg
Flash Point:146.6°C
Density:1.201g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:196.0291072
Heavy Atom Count:13
Complexity:191

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Cl)C=CC=O
Isomeric SMILES:COC1=C(C=C(C=C1)Cl)/C=C/C=O

Technology Process of 3-(5-Chloro-2-methoxyphenyl)prop-2-enal

There total 2 articles about 3-(5-Chloro-2-methoxyphenyl)prop-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 6628-07-5
N-allyl-N-methylaniline

: 52807-27-9
4-chloro-2-iodo-1-methoxybenzene

: 33538-90-8
5-chloro-2-methoxycinnamaldehyde

Guidance literature:: With tetrabutylammomium bromide; sodium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 120 ℃; for 8h; in air;
DOI:10.1039/b917782e

Reference yield:

: 7035-09-8
5-chloro-2-methoxybenzaldehyde

: 109-92-2,25104-37-4
ethyl vinyl ether

: 33538-90-8
5-chloro-2-methoxycinnamaldehyde

Guidance literature:: Multistep reaction; (i) HC(OEt)3, H₃PO₄, (ii) /BRN= 605351/, ZnCl₂, AcOEt, (iii) aq. NaOAc, AcOH;
DOI:10.1002/jps.2600600815