3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan

Base Information

Chemical Name:3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan
CAS No.:83631-17-8
Molecular Formula:C15H22O
Molecular Weight:0
Hs Code.:
Mol file:83631-17-8.mol

Synonyms:dihydropallescensin-2;penlanpallescensin;3-[2-((S)-2,2-Dimethyl-6-methylene-cyclohexyl)-ethyl]-furan;

Suppliers and Price of 3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan

Chemical Property:

PSA：13.14000
LogP:4.59470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan

There total 7 articles about 3-[2-[(1S)-2,2-Dimethyl-6-methylenecyclohexyl]ethyl]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 111931-31-8
(S)-2-(2-Iodo-ethyl)-1,1-dimethyl-3-methylene-cyclohexane

: 53101-93-2
3-furyllithium

: 83631-17-8
(+)-dihydropallescensin-2

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95903-3

Reference yield:

: 112243-60-4
(1'S)-2-(2',2'-dimethyl-6'-methylene-cyclohexyl)-ethanol

: 83631-17-8
(+)-dihydropallescensin-2

Guidance literature:: Multi-step reaction with 3 steps

1: EtN₃ / CH₂Cl₂

2: NaI / acetone / Heating

3: 83 percent / HMPA / tetrahydrofuran

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium iodide; ethyl azide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)95903-3

Reference yield:

: 782474-36-6
((S)-2,2-Dimethyl-6-methylene-cyclohexyl)-acetic acid

: 83631-17-8
(+)-dihydropallescensin-2

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / LiAlH₄ / diethyl ether / 25 °C

2: EtN₃ / CH₂Cl₂

3: NaI / acetone / Heating

4: 83 percent / HMPA / tetrahydrofuran

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sodium iodide; ethyl azide; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)95903-3