Technology Process of 2-Naphthalenamine,
8-bromo-1,2,3,4-tetrahydro-5-methyl-N-(phenylmethyl)-
There total 4 articles about 2-Naphthalenamine,
8-bromo-1,2,3,4-tetrahydro-5-methyl-N-(phenylmethyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bromine; potassium carbonate / water
2: thionyl chloride / dichloromethane / 30 °C / Reflux
3: aluminum (III) chloride
4: sodium tris(acetoxy)borohydride
With
aluminum (III) chloride; thionyl chloride; bromine; sodium tris(acetoxy)borohydride; potassium carbonate;
In
dichloromethane; water;
3: Friedel Crafts alkylation;
DOI:10.1021/jo300277y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 30 °C / Reflux
2: aluminum (III) chloride
3: sodium tris(acetoxy)borohydride
With
aluminum (III) chloride; thionyl chloride; sodium tris(acetoxy)borohydride;
In
dichloromethane;
2: Friedel Crafts alkylation;
DOI:10.1021/jo300277y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aluminum (III) chloride
2: sodium tris(acetoxy)borohydride
With
aluminum (III) chloride; sodium tris(acetoxy)borohydride;
1: Friedel Crafts alkylation;
DOI:10.1021/jo300277y