3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one

Base Information

• Chemical Name: 3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one
• CAS No.: 634615-48-8
• Molecular Formula: C15H11BrO2
• Molecular Weight: 303.155
• DSSTox Substance ID: DTXSID201217084

Synonyms:3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one;DTXSID201217084;AKOS034379900;634615-48-8

Chemical Property of 3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 301.99424
• Heavy Atom Count: 18
• Complexity: 306

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=CC(=O)C2=CC=C(C=C2)O)Br

Technology Process of 3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one

There total 1 articles about 3-(2-Bromophenyl)-1-(4-hydroxyphenyl)-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

ortho-bromobenzaldehyde (6630-33-7) + 4-Hydroxyacetophenone (99-93-4) → 3-(2-bromophenyl)-1-(4-hydroxyphenyl)propenone (634615-48-8)

Guidance literature:

4-Hydroxyacetophenone; With sodium hydroxide; In methanol; for 0.166667h; Cooling with ice;

ortho-bromobenzaldehyde; With sodium hydroxide; In methanol; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2009.10.023

Reference yield: 98.0%

Nicotinic acid hydrazide (553-53-7) + 3-(2-bromophenyl)-1-(4-hydroxyphenyl)propenone (634615-48-8) → [5-(2-bromophenyl)-3-(4-hydroxyphenyl)-4,5-dihydropyrazol-1-yl]pyridin-3-yl-methanone (1214751-12-8)

Guidance literature:

In butan-1-ol; for 8h; Reflux;

DOI:10.1016/j.ejmech.2009.10.023

Reference yield: 77.0%

3-(2-bromophenyl)-1-(4-hydroxyphenyl)propenone (634615-48-8) + 2-amino-benzenethiol (137-07-5) → 4-(2-(2-bromophenyl)-2,3-dihydrobenzo[b][1,4]thiazepine-4-yl)phenol

Guidance literature:

With hydrogenchloride; sodium sulfate; In ethanol; water; Reflux;

DOI:10.1016/j.ejmech.2016.09.069

upstream raw materials:

ortho-bromobenzaldehyde

4-Hydroxyacetophenone

Downstream raw materials:

[5-(2-bromophenyl)-3-(4-hydroxyphenyl)-4,5-dihydropyrazol-1-yl]pyridin-3-yl-methanone

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