N,2-Dihydroxy-5-methoxybenzamide

Base Information

• Chemical Name: N,2-Dihydroxy-5-methoxybenzamide
• CAS No.: 63482-89-3
• Molecular Formula: C₈H₉NO₄
• Molecular Weight: 183.164
• DSSTox Substance ID: DTXSID30494458
• Wikidata: Q82341832

Synonyms:N,2-Dihydroxy-5-methoxybenzamide;63482-89-3;SCHEMBL1436731;5-methoxy-salicylhydroxamic acid;DTXSID30494458;AKOS009125868

Chemical Property of N,2-Dihydroxy-5-methoxybenzamide

Chemical Property:

• XLogP3: 0.9
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 183.05315777
• Heavy Atom Count: 13
• Complexity: 185

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=C(C=C1)O)C(=O)NO

Technology Process of N,2-Dihydroxy-5-methoxybenzamide

There total 2 articles about N,2-Dihydroxy-5-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 5-methoxy-2-hydroxybenzoate (2905-82-0) → 2,N-dihydroxy-5-methoxy-benzamide (63482-89-3)

Guidance literature:

With hydroxylamine;

Reference yield:

→ 2,N-dihydroxy-5-methoxy-benzamide (63482-89-3)

Guidance literature:

entspr. Methylester, NH2OH;

Reference yield:

2,N-dihydroxy-5-methoxy-benzamide (63482-89-3) → 5-Methoxy-3-hydroxy-1,2-benzisoxazol (66607-95-2)

Guidance literature:

Multistep reaction; (i) 1H,1'H-1,1'-carbonyl-bis-imidazole, THF, (ii) aq. HCl;

upstream raw materials:

methyl 5-methoxy-2-hydroxybenzoate

Downstream raw materials:

5-Methoxy-3-hydroxy-1,2-benzisoxazol

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