Benzo[c]phenanthren-4-ol

Base Information

Chemical Name:Benzo[c]phenanthren-4-ol
CAS No.:22717-96-0
Molecular Formula:C₁₈H₁₂O
Molecular Weight:244.293
Hs Code.:
NSC Number:171264
DSSTox Substance ID:DTXSID70177253
Wikidata:Q83047565

Synonyms:Benzo[c]phenanthren-4-ol;Benzo(c)phenanthren-4-ol;22717-96-0;NSC171264;NSC 171264;DTXSID70177253;NSC-171264

Suppliers and Price of Benzo[c]phenanthren-4-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzo[c]phenanthren-4-ol

Chemical Property:

Vapor Pressure:1.5E-10mmHg at 25°C
Boiling Point:498.2°Cat760mmHg
Flash Point:240.4°C
Density:1.284g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:244.088815002
Heavy Atom Count:19
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C4=C(C=C3)C(=CC=C4)O

Technology Process of Benzo[c]phenanthren-4-ol

There total 7 articles about Benzo[c]phenanthren-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4216-68-6
4-methoxybenzophenanthrene

: 22717-96-0
4-hydroxybenzophenanthrene

Guidance literature:: With boron tribromide; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/jo00301a054

Reference yield:

4-hydroxybenzophenantrene acetate: 80285-05-8
4-hydroxybenzophenantrene acetate

: 22717-96-0
4-hydroxybenzophenanthrene

Guidance literature:: With hydrogenchloride; In methanol; for 24h; Yield given; Ambient temperature;
DOI:10.1021/jo00340a005

Reference yield:

: 73093-16-0
1,2-dihydrobenzophenanthrene

: 22717-96-0
4-hydroxybenzophenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / lithium acetate / acetic acid / 1.5 h / Ambient temperature

2: 74 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Heating

3: 40 percent / sodium methoxide / tetrahydrofuran / 18 h / 0 °C

4: benzoic acid / Ambient temperature

With N-Bromosuccinimide; lithium acetate; sodium methylate; benzoic acid; In tetrahydrofuran; tetrachloromethane; acetic acid;