Benzaldehyde, 4-[5-[4-(2,2-dimethylpropyl)phenyl]-1,2,4-oxadiazol-3-yl]-

Base Information

Chemical Name:Benzaldehyde, 4-[5-[4-(2,2-dimethylpropyl)phenyl]-1,2,4-oxadiazol-3-yl]-
CAS No.:635702-01-1
Molecular Formula:C20H20N2O2
Molecular Weight:320.391
Hs Code.:

Synonyms:

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Chemical Property of Benzaldehyde, 4-[5-[4-(2,2-dimethylpropyl)phenyl]-1,2,4-oxadiazol-3-yl]-

Chemical Property:

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Technology Process of Benzaldehyde, 4-[5-[4-(2,2-dimethylpropyl)phenyl]-1,2,4-oxadiazol-3-yl]-

There total 5 articles about Benzaldehyde, 4-[5-[4-(2,2-dimethylpropyl)phenyl]-1,2,4-oxadiazol-3-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-89-5
4-Cyanobenzyl alcohol

: 635702-01-1
4-(5-(4-(2,2-dimethylpropyl)phenyl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / hydroxyamine hydrochloride; sodium bicarbonate / methanol / 5 h / Heating

2.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole hydrate / dimethylformamide / 20 °C

2.2: dimethylformamide / 140 °C

3.1: oxalyl chloride; DMSO; N,N-diisopropylethylamine / CH₂Cl₂ / -78 - 20 °C

With oxalyl dichloride; hydroxylamine hydrochloride; sodium hydrogencarbonate; dimethyl sulfoxide; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0503244

Reference yield:

: (4-{5-[4-(2,2-dimethyl-propyl)-phenyl]-[1,2,4]oxadiazol-3-yl}-phenyl)-methanol

: 635702-01-1
4-(5-(4-(2,2-dimethylpropyl)phenyl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jm0503244

Reference yield:

: 635702-23-7
(E)-N′-hydroxy-4-(hydroxymethyl)benzimidamide

: 635702-01-1
4-(5-(4-(2,2-dimethylpropyl)phenyl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole hydrate / dimethylformamide / 20 °C

1.2: dimethylformamide / 140 °C

2.1: oxalyl chloride; DMSO; N,N-diisopropylethylamine / CH₂Cl₂ / -78 - 20 °C

With oxalyl dichloride; dimethyl sulfoxide; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0503244