Ethanedione, diphenyl-, mono[[1-methyl-2-(triphenylphosphoranylidene)ethylidene]hydrazone]

Base Information

• Chemical Name: Ethanedione, diphenyl-, mono[[1-methyl-2-(triphenylphosphoranylidene)ethylidene]hydrazone]
• CAS No.: 63570-25-2
• Molecular Formula: C35H29N2OP
• Molecular Weight: 524.602

Synonyms:(2-(2-OXO-1,2-DIPHENYLETHYLIDENEHYDRAZINYLIDENE)PROPYLIDENE)TRIPHENYLPHOSPHORANE;

Chemical Property of Ethanedione, diphenyl-, mono[[1-methyl-2-(triphenylphosphoranylidene)ethylidene]hydrazone]

Chemical Property:

• PSA: 51.60000
• LogP: 6.53080

Purity/Quality:

(2-(2-OXO-1,2-DIPHENYLETHYLIDENEHYDRAZINYLIDENE)PROPYLIDENE)TRIPHENYLPHOSPHORANE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanedione, diphenyl-, mono[[1-methyl-2-(triphenylphosphoranylidene)ethylidene]hydrazone]

There total 1 articles about Ethanedione, diphenyl-, mono[[1-methyl-2-(triphenylphosphoranylidene)ethylidene]hydrazone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-{[1-Methyl-2-(triphenyl-λ5-phosphanylidene)-eth-(E)-ylidene]-hydrazono}-1,2-diphenyl-ethanone (63570-25-2)

Guidance literature:

Verb.14, Verb.22;

DOI:10.1021/jo00443a012

Reference yield: 87.0%

4,5-Dihydro-naphtho[1,2-b]furan-2,3-dione (55991-73-6) + 2-{[1-Methyl-2-(triphenyl-λ5-phosphanylidene)-eth-(Z)-ylidene]-hydrazono}-1,2-diphenyl-ethanone (63570-25-2) → 2-[2-{[2-Oxo-1,2-diphenyl-eth-(E)-ylidene]-hydrazono}-prop-(Z)-ylidene]-4,5-dihydro-naphtho[1,2-b]furan-3-one (107353-37-7)

Guidance literature:

In benzene; for 15h; Ambient temperature;

DOI:10.1021/jo00383a029

Reference yield: 85.0%

4-Methyl-5-phenyl-2,3-dihydrofuran-2,3-dione (55991-71-4) + 2-{[1-Methyl-2-(triphenyl-λ5-phosphanylidene)-eth-(Z)-ylidene]-hydrazono}-1,2-diphenyl-ethanone (63570-25-2) → 4-Methyl-2-[2-{[2-oxo-1,2-diphenyl-eth-(E)-ylidene]-hydrazono}-prop-(Z)-ylidene]-5-phenyl-furan-3-one (107353-18-4)

Guidance literature:

In benzene; for 15h; Ambient temperature;

DOI:10.1021/jo00383a029

Downstream raw materials:

4-Benzoyl-2-methyl-4-phenyl-5-oxa-3,3a-diaza-benzo[e]azulen-6-one

4-Methyl-2-[2-{[2-oxo-1,2-diphenyl-eth-(E)-ylidene]-hydrazono}-prop-(Z)-ylidene]-5-phenyl-furan-3-one

2-[2-{[2-Oxo-1,2-diphenyl-eth-(E)-ylidene]-hydrazono}-prop-(Z)-ylidene]-4,5-dihydro-naphtho[1,2-b]furan-3-one

8-benzoyl-6,8-diphenyl-2-methyl-4H,8H-pyrazolo<1,5-c><1,3>oxazepin-4-one

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