3,7-Di(benzenesulfonyl)-10H-phenoxazine

Base Information

• Chemical Name: 3,7-Di(benzenesulfonyl)-10H-phenoxazine
• CAS No.: 63720-25-2
• Molecular Formula: C₂₄H₁₇NO₅S₂
• Molecular Weight: 463.535
• DSSTox Substance ID: DTXSID50493463
• Wikidata: Q82340164
• Mol file: 63720-25-2.mol

Synonyms:3,7-Di(benzenesulfonyl)-10H-phenoxazine;63720-25-2;DTXSID50493463;3,7-di(phenylsulfonyl)phenoxazine

Chemical Property of 3,7-Di(benzenesulfonyl)-10H-phenoxazine

Chemical Property:

• XLogP3: 4.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 463.05481499
• Heavy Atom Count: 32
• Complexity: 780

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)S(=O)(=O)C2=CC3=C(C=C2)NC4=C(O3)C=C(C=C4)S(=O)(=O)C5=CC=CC=C5

Technology Process of 3,7-Di(benzenesulfonyl)-10H-phenoxazine

There total 3 articles about 3,7-Di(benzenesulfonyl)-10H-phenoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenoxazine (135-67-1) → 3,7-bis-benzenesulfonyl-10H-phenoxazine (63720-25-2)

Guidance literature:

Multi-step reaction with 2 steps

1: FeCl₃ / acetic acid

2: FeCl₃ / acetic acid / 20 h / Heating

With iron(III) chloride; In acetic acid;

DOI:10.1007/BF00473193

Reference yield:

sodium benzenesulfonate (873-55-2) → 3,7-bis-benzenesulfonyl-10H-phenoxazine (63720-25-2)

Guidance literature:

Multi-step reaction with 2 steps

1: FeCl₃ / acetic acid

2: FeCl₃ / acetic acid / 20 h / Heating

With iron(III) chloride; In acetic acid;

DOI:10.1007/BF00473193

Reference yield:

3-(phenylsulfonyl)-10H-phenoxazine (63673-66-5) + sodium benzenesulfonate (873-55-2) → 3,7-bis-benzenesulfonyl-10H-phenoxazine (63720-25-2)

Guidance literature:

With iron(III) chloride; In acetic acid; for 20h; Heating;

DOI:10.1007/BF00473193

upstream raw materials:

3-(phenylsulfonyl)-10H-phenoxazine

sodium benzenesulfonate

phenoxazine