N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine

Base Information

• Chemical Name: N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine
• CAS No.: 63725-50-8
• Molecular Formula: C₈H₁₀N₄
• Molecular Weight: 162.194
• Hs Code.: 2933998090
• DSSTox Substance ID: DTXSID201245936

Synonyms:N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine;63725-50-8;DTXSID201245936;CS-0454433;1h-pyrazolo[3,4-b]pyridin-6-amine,n,n-dimethyl-;N,N-dimethyl-2H-pyrazolo[3,4-b]pyridin-6-amine

Chemical Property of N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine

Chemical Property:

• PSA: 44.81000
• LogP: 1.02390
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 162.090546336
• Heavy Atom Count: 12
• Complexity: 159

Purity/Quality:

98%+ ^*data from raw suppliers

N,N-dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CN(C)C1=NC2=C(C=C1)C=NN2

Technology Process of N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine

There total 2 articles about N,N-Dimethyl-1H-pyrazolo[3,4-b]pyridin-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

6-(dimethylamino)-2-fluoropyridine-3-carboxaldehyde N-aceylhydrazone → 6-(dimethylamino)-1H-pyrazole<3,4-b>pyridine (63725-50-8)

Guidance literature:

With hydrazine hydrate; at 90 ℃; for 0.25h;

DOI:10.1002/jhet.5570340314

Reference yield:

2-fluoro-6-dimethylaminopyridine-3-carbaldehyde (193481-63-9) → 6-(dimethylamino)-1H-pyrazole<3,4-b>pyridine (63725-50-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / ethanol / Ambient temperature

2: 88 percent / hydrazine hydrate / 0.25 h / 90 °C

With hydrazine hydrate; In ethanol;

DOI:10.1002/jhet.5570340314

upstream raw materials:

2-fluoro-6-dimethylaminopyridine-3-carbaldehyde

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