Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester

Base Information

Chemical Name:Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester
CAS No.:63744-96-7
Molecular Formula:C28H34O9
Molecular Weight:514.573
Hs Code.:

Synonyms:

Suppliers and Price of Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester

There total 14 articles about Benzoic acid, 2,4-dihydroxy-6-(2-oxoheptyl)-, 4-carboxy-3-hydroxy-5-(2-oxoheptyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: benzyl 4-O-demethylmicrophyllinate

: 63744-96-7
4-O-demethylmicrophyllinic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 3h;

Reference yield:

: 62054-00-6
3,3-(ethylenedioxy)octan-1-ol

: 63744-96-7
4-O-demethylmicrophyllinic acid

Guidance literature:: Multi-step reaction with 10 steps

1: 60 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

2: 69 percent / toluene / 20 h / Heating

3: 55 percent / ethanol / 24 h / Heating

4: acetic acid / 0.5 h / Heating

6: 38 percent / phenylmethanol / 24 h / 130 °C

7: 97 percent / p-toluenesulfonic acid / acetone / 10 h / Ambient temperature

8: 12 percent / dicyclohexylcarbodiimide / diethyl ether / 2 h / Ambient temperature

9: p-toluenesulfonic acid / acetone / 10 h / Ambient temperature

10: H₂ / 10percent Pd/C / ethyl acetate / 2 h

With hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; acetic acid; ethyl acetate; acetone; toluene; benzyl alcohol;

Reference yield:

: 61857-33-8
ethyl 3,3-(ethylenedioxy)octanoate

: 63744-96-7
4-O-demethylmicrophyllinic acid

Guidance literature:: Multi-step reaction with 11 steps

1: 82 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating

2: 60 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

3: 69 percent / toluene / 20 h / Heating

4: 55 percent / ethanol / 24 h / Heating

5: acetic acid / 0.5 h / Heating

7: 38 percent / phenylmethanol / 24 h / 130 °C

8: 97 percent / p-toluenesulfonic acid / acetone / 10 h / Ambient temperature

9: 12 percent / dicyclohexylcarbodiimide / diethyl ether / 2 h / Ambient temperature

10: p-toluenesulfonic acid / acetone / 10 h / Ambient temperature

11: H₂ / 10percent Pd/C / ethyl acetate / 2 h

With lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; acetic acid; ethyl acetate; acetone; toluene; benzyl alcohol;