Cyclohexanol, 2-(1,3-benzodioxol-5-yl)-, trans-

Base Information

Chemical Name:Cyclohexanol, 2-(1,3-benzodioxol-5-yl)-, trans-
CAS No.:63765-10-6
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanol, 2-(1,3-benzodioxol-5-yl)-, trans-

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Technology Process of Cyclohexanol, 2-(1,3-benzodioxol-5-yl)-, trans-

There total 1 articles about Cyclohexanol, 2-(1,3-benzodioxol-5-yl)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63765-10-6,108881-50-1
(1S,2R)-2-Benzo[1,3]dioxol-5-yl-cyclohexanol

Guidance literature:: aus 5-Brom-benzo-1,3-dioxol, Cyclohexanon/ Py.;
DOI:10.1021/jo00862a025

Reference yield: 51.0%

: 63765-10-6,108881-50-1
(1S,2R)-2-Benzo[1,3]dioxol-5-yl-cyclohexanol

: cis-2-(benzo[d][1,3]dioxol-5-yl)cyclohexylamine

Guidance literature:: (1S,2R)-2-Benzo[1,3]dioxol-5-yl-cyclohexanol; With phthalimide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

With hydrazine hydrate; In ethanol; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201604440

Reference yield:

: 63765-10-6,108881-50-1
(1S,2R)-2-Benzo[1,3]dioxol-5-yl-cyclohexanol

: 87961-41-9
1,3-benzodioxole-5-δ-ketopentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

1.2: 2 h / Inert atmosphere; Reflux

2.1: oxygen; rose bengal / 1,4-dioxane / 24 h / 25 °C / Irradiation

With phthalimide; di-isopropyl azodicarboxylate; rose bengal; oxygen; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/chem.201604440