Acrylic acid 3-bromopropyl ester

Base Information

• Chemical Name: Acrylic acid 3-bromopropyl ester
• CAS No.: 64046-90-8
• Molecular Formula: C6H9BrO2
• Molecular Weight: 193.04

Synonyms:2-propenoic acid, 3-bromopropyl ester;acrylic acid-(3-bromo-propyl ester);1-Acryloyloxy-3-brom-propan;Acrylsaeure-(3-brom-propylester);Acrylic acid 3-bromo-propyl ester;

Chemical Property of Acrylic acid 3-bromopropyl ester

Chemical Property:

• Boiling Point: 96 °C (18 mmHg)
• PSA: 26.30000
• LogP: 1.50060

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acrylic acid 3-bromopropyl ester

There total 2 articles about Acrylic acid 3-bromopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

acryloyl chloride (814-68-6,25189-84-8) + 1-bromo-3-propanol (627-18-9) → 3-bromopropyl prop-2-enoate (64046-90-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

ethyl acrylate (140-88-5,9003-32-1) + 1-bromo-3-propanol (627-18-9) → 3-bromopropyl prop-2-enoate (64046-90-8)

Guidance literature:

in Gegenwart von Saeure;

DOI:10.1021/ja01167a116

Reference yield: 89.0%

3-bromopropyl prop-2-enoate (64046-90-8) + diazodiphenylmethane (908093-98-1) → 2,2-diphenylcyclopropanecarboxylic acid bromopropyl ester

Guidance literature:

In ethyl acetate; at 70 ℃; for 2h;

upstream raw materials:

ethyl acrylate

1-bromo-3-propanol

acryloyl chloride

Downstream raw materials:

3-(4-{(E)-2-[2-(hydroxymethyl)-4-nitrophenyl]vinyl}phenoxy)propyl acrylate

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