1,3(2H)-Pyridinedicarboxylic acid, 4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-, 1-(1,1-dimethylethyl) 3-methyl ester

Base Information

Chemical Name:1,3(2H)-Pyridinedicarboxylic acid, 4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-, 1-(1,1-dimethylethyl) 3-methyl ester
CAS No.:642487-32-9
Molecular Formula:C27H43NO5Si
Molecular Weight:489.728
Hs Code.:

1,3(2H)-Pyridinedicarboxylic acid,
4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-,
1-(1,1-dimethylethyl) 3-methyl ester

Synonyms:

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Chemical Property of 1,3(2H)-Pyridinedicarboxylic acid, 4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-, 1-(1,1-dimethylethyl) 3-methyl ester

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Technology Process of 1,3(2H)-Pyridinedicarboxylic acid, 4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-, 1-(1,1-dimethylethyl) 3-methyl ester

There total 1 articles about 1,3(2H)-Pyridinedicarboxylic acid, 4-[4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]phenyl]-5,6-dihydro-, 1-(1,1-dimethylethyl) 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 161491-25-4
1-tert-butyl 3-methyl 4-(((trifluoromethyl)sulfonyl)oxy)-5,6-dihydropyridine-1,3(2H)-dicarboxylate

: 153993-80-7
[3-(4-bromophenyl)propoxy](tert-butyl)dimethylsilane

: 642487-32-9
4-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester

Guidance literature:: [3-(4-bromophenyl)propoxy](tert-butyl)dimethylsilane; With n-butyllithium; zinc(II) chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h;

1-tert-butyl 3-methyl 4-(((trifluoromethyl)sulfonyl)oxy)-5,6-dihydropyridine-1,3(2H)-dicarboxylate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 20 ℃; for 0.333333h;

Reference yield: 84.0%

: 642487-32-9
4-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester

: 642487-34-1
4-[4-(3-hydroxypropyl)phenyl]-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 6h;

Reference yield:

: 642487-32-9
4-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester

: 1007393-52-3
C₂₀H₂₇NO₅

Guidance literature:: 4-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester; With sodium hydroxide; water; In tetrahydrofuran; dimethyl sulfoxide; at 50 ℃; for 7h;

With hydrogenchloride; In tetrahydrofuran; water; dimethyl sulfoxide; pH=2;