3-Pyridinecarboxamide, N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl )methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)-

Base Information

Chemical Name:3-Pyridinecarboxamide, N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl )methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)-
CAS No.:642487-48-7
Molecular Formula:C39H43ClN2O4
Molecular Weight:639.234
Hs Code.:

3-Pyridinecarboxamide,
N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl
)methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)-

Synonyms:

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Chemical Property of 3-Pyridinecarboxamide, N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl )methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)-

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Technology Process of 3-Pyridinecarboxamide, N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl )methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)-

There total 1 articles about 3-Pyridinecarboxamide, N-[2-(2-chlorophenyl)ethyl]-1,2,5,6-tetrahydro-4-[4-[3-[(2-methoxyphenyl )methoxy]propoxy]phenyl]-N-methyl-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 642487-30-7
1-benzyl-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester

: 52516-17-3
2-(2-chlorochlorophenyl)-N-methylethanamine

: 642487-48-7
1-benzyl-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydropyridine-3-carboxylic acid [2-(2-chlorophenyl)ethyl]methylamide

Guidance literature:: 1-benzyl-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester; With sodium hydroxide; In ethanol; at 20 - 60 ℃; for 9h;

With hydrogenchloride; In ethanol; water; at 20 ℃; pH=7;

2-(2-chlorochlorophenyl)-N-methylethanamine; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; benzotriazol-1-ol; In chloroform; at 20 ℃; for 4h;

Reference yield:

: 642487-48-7
1-benzyl-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydropyridine-3-carboxylic acid [2-(2-chlorophenyl)ethyl]methylamide

: 4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydropyridine-3-carboxylic acid [2-(2-chlorophenyl)ethyl]methylamide

Guidance literature:: 1-benzyl-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}-1,2,5,6-tetrahydropyridine-3-carboxylic acid [2-(2-chlorophenyl)ethyl]methylamide; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; at 20 ℃; for 7h; Heating / reflux;

In methanol; water;