2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline

Base Information

Chemical Name:2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline
CAS No.:64388-18-7
Molecular Formula:C15H10N2O3
Molecular Weight:266.256
Hs Code.:
DSSTox Substance ID:DTXSID90494671
Wikidata:Q82342211

Synonyms:64388-18-7;2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline;DTXSID90494671

Suppliers and Price of 2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:266.06914219
Heavy Atom Count:20
Complexity:350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC(=[N+]2[O-])C3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of 2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline

There total 4 articles about 2-(4-Nitrophenyl)-1-oxo-1lambda~5~-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1613-37-2
Quinoline N-oxide

: 100-01-6,104810-17-5
4-nitro-aniline

: 64388-18-7
2-(4-nitrophenyl)quinoline 1-oxide

Guidance literature:: With tert.-butylnitrite; copper(II) acetate pentahydrate; calcium carbonate; In water; acetone; at 50 ℃; for 1.5h; regioselective reaction; Schlenk technique;
DOI:10.1016/j.tet.2017.03.009

Reference yield:

: 64388-23-4
2-(4-nitrophenyl)quinoline

: 64388-18-7
2-(4-nitrophenyl)quinoline 1-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; Sealed tube; Schlenk technique;
DOI:10.1021/acs.joc.8b02042

Reference yield:

: 91-22-5
quinoline

: 64388-18-7
2-(4-nitrophenyl)quinoline 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium perborate tetrahydrate / acetic acid / 40 °C

2: tert.-butylnitrite / acetonitrile / 18 h / 20 - 40 °C

With tert.-butylnitrite; sodium perborate tetrahydrate; In acetic acid; acetonitrile;
DOI:10.1016/j.tet.2018.05.066