4-(Phenylmethoxy)azobenzene

Base Information

• Chemical Name: 4-(Phenylmethoxy)azobenzene
• CAS No.: 75365-76-3
• Molecular Formula: C13H12N2O
• Molecular Weight: 288.349
• European Community (EC) Number: 278-192-2
• DSSTox Substance ID: DTXSID801260350
• Nikkaji Number: J307.561C
• Mol file: 75365-76-3.mol

Synonyms:4-(Phenylmethoxy)azobenzene;75365-76-3;4-Benzyloxyazobenzene;phenyl-(4-phenylmethoxyphenyl)diazene;EINECS 278-192-2;Phenyl[4-(phenylmethoxy)phenyl]diazene;1-Phenyl-2-[4-(phenylmethoxy)phenyl]diazene;SDKQJMOEGSAXET-UHFFFAOYSA-N;DTXSID801260350;AKOS030255371;benzyl 4-[(E)-phenyldiazenyl]phenyl ether;NS00060914;(E)-[4-(BENZYLOXY)PHENYL](PHENYL)DIAZENE

Chemical Property of 4-(Phenylmethoxy)azobenzene

Chemical Property:

• Vapor Pressure: 0.000788mmHg at 25°C
• Boiling Point: 315.9°Cat760mmHg
• Flash Point: 118.7°C
• PSA: 33.95000
• Density: 1.05g/cm³
• LogP: 5.68100
• XLogP3: 5.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 288.126263138
• Heavy Atom Count: 22
• Complexity: 324

Purity/Quality:

99% ^*data from raw suppliers

4-Benzyloxyazobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)COC2=CC=C(C=C2)N=NC3=CC=CC=C3
• Uses: Intermediate in the preparation of Oxyphenbutazone.

Technology Process of 4-(Phenylmethoxy)azobenzene

There total 2 articles about 4-(Phenylmethoxy)azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloride (100-44-7) + 4-hydroxyazobenzene (1689-82-3) → (4-benzyloxy-phenyl)-phenyl-diazene (75365-76-3)

Guidance literature:

With ethanol; sodium ethanolate;

Reference yield:

→ (4-benzyloxy-phenyl)-phenyl-diazene (75365-76-3)

Guidance literature:

4-Hydroxy-azobenzol, Na, Benzylchlorid;

Reference yield:

(4-benzyloxy-phenyl)-phenyl-diazene (75365-76-3) → 1-(4-benzyloxyphenyl)-2-phenylhydrazine (93942-75-7)

Guidance literature:

With zinc;

DOI:10.1002/hlca.19570400218

upstream raw materials:

benzyl chloride

4-hydroxyazobenzene

Downstream raw materials:

1-(4-benzyloxyphenyl)-2-phenylhydrazine