3,4-Diacetoxybenzylidene diacetate

Base Information

Chemical Name:3,4-Diacetoxybenzylidene diacetate
CAS No.:65479-32-5
Molecular Formula:C15H16 O8
Molecular Weight:324.28
Hs Code.:2918990090
DSSTox Substance ID:DTXSID80215796
Nikkaji Number:J555.678C
Wikidata:Q83091893
Mol file:65479-32-5.mol

Synonyms:3,4-diAcBz diAc;3,4-diacetoxybenzylidene diacetate

Suppliers and Price of 3,4-Diacetoxybenzylidene diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(ACETYLOXY)-4-[BIS(ACETYLOXY)METHYL]PHENYL ACETATE 95.00%
5MG
$ 501.16

Total 4 raw suppliers

Chemical Property of 3,4-Diacetoxybenzylidene diacetate

Chemical Property:

Vapor Pressure:1.52E-07mmHg at 25°C
Boiling Point:428.4°C at 760 mmHg
Flash Point:188.7°C
PSA：105.20000
Density:1.272g/cm³
LogP:1.66200
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:9
Exact Mass:324.08451746
Heavy Atom Count:23
Complexity:456

Purity/Quality:

99% ^*data from raw suppliers

2-(ACETYLOXY)-4-[BIS(ACETYLOXY)METHYL]PHENYL ACETATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=C(C=C(C=C1)C(OC(=O)C)OC(=O)C)OC(=O)C

Technology Process of 3,4-Diacetoxybenzylidene diacetate

There total 4 articles about 3,4-Diacetoxybenzylidene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-24-7
acetic anhydride

: 139-85-5
3,4-dihydroxybenzaldehyde

: 65479-32-5
1,2-diacetoxy-4-diacetoxymethyl-benzene

Guidance literature:: With silica-bonded S-sulfonic acid; at 20 ℃; for 0.0333333h;
DOI:10.1016/j.tetlet.2009.04.096

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 65479-32-5
1,2-diacetoxy-4-diacetoxymethyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: aq.-ethanolic KOH

2: aqueous HClO₄

With potassium hydroxide; perchloric acid;
DOI:10.1039/jr9510000522