Technology Process of 4,8-Dimethylphenanthro[3,2-b]furan-7,11-dione
There total 5 articles about 4,8-Dimethylphenanthro[3,2-b]furan-7,11-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; triphenylphosphine; potassium carbonate / toluene / 17 h / 110 °C / Darkness
1.2: 2 h / 80 °C
2.1: ammonium acetate / 0.25 h / 110 °C / Sealed tube; Microwave irradiation
With
ammonium acetate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
toluene;
1.1: |Heck Reaction;
DOI:10.1371/journal.pone.0240231
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium carbonate; dihydrogen peroxide / tetrahydrofuran; water / 5 h / 20 °C
2.1: iron(III) chloride hexahydrate / water; methanol / 5 h / 20 °C
3.1: ammonium peroxydisulfate / water; acetonitrile / 2.5 h / 85 °C / Darkness
4.1: palladium diacetate; triphenylphosphine; potassium carbonate / toluene / 17 h / 110 °C / Darkness
4.2: 2 h / 80 °C
5.1: ammonium acetate / 0.25 h / 110 °C / Sealed tube; Microwave irradiation
With
ammonium peroxydisulfate; iron(III) chloride hexahydrate; ammonium acetate; dihydrogen peroxide; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; water; toluene; acetonitrile;
1.1: |Baeyer-Villiger Ketone Oxidation / 4.1: |Heck Reaction;
DOI:10.1371/journal.pone.0240231
