4'-t-Butyl-4-dimethylaminoazobenzene

Base Information

• Chemical Name: 4'-t-Butyl-4-dimethylaminoazobenzene
• CAS No.: 24596-41-6
• Molecular Formula: C₁₈H₂₃N₃
• Molecular Weight: 281.401
• Hs Code.: 2927000090
• NSC Number: 170580
• Nikkaji Number: J33.764A
• Mol file: 24596-41-6.mol

Synonyms:4'-t-Butyl-4-dimethylaminoazobenzene;24596-41-6;NSC 170580;BRN 1883795;p-((p-t-Butylphenyl)azo)-N,N-dimethylaniline;ANILINE, p-((p-(t-BUTYL)PHENYL)AZO)-N,N-DIMETHYL-;Aniline, p-((p-tert-butylphenyl)azo)-N,N-dimethyl-;Benzenamine, 4-((4-(1,1-dimethylethyl)phenyl)azo)-N,N-dimethyl-;Aniline, p-[(p-tert-butylphenyl)azo]-N,N-dimethyl-;Benzenamine, 4-[[4-(1,1-dimethylethyl)phenyl]azo]-N,N-dimethyl-;NSC170580;NSC-170580;LS-19636;4-[[p-(tert-Butyl)phenyl]azo]-N,N-dimethylaniline;Benzenamine,1-dimethylethyl)phenyl]azo]-N,N-dimethyl-

Chemical Property of 4'-t-Butyl-4-dimethylaminoazobenzene

Chemical Property:

• Vapor Pressure: 3.91E-07mmHg at 25°C
• Refractive Index: 1.5480 (estimate)
• Boiling Point: 416.1°Cat760mmHg
• Flash Point: 205.5°C
• PSA: 27.96000
• Density: 0.98g/cm³
• LogP: 5.46550
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 281.189197746
• Heavy Atom Count: 21
• Complexity: 327

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)C1=CC=C(C=C1)N=NC2=CC=C(C=C2)N(C)C

Technology Process of 4'-t-Butyl-4-dimethylaminoazobenzene

There total 3 articles about 4'-t-Butyl-4-dimethylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-tert-butylphenyl)diazonium tetrafluoroborate (52436-75-6) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → [4-(4-tert-Butyl-phenylazo)-phenyl]-dimethyl-amine (24596-41-6)

Guidance literature:

In 1,2-dichloro-ethane; at 25 ℃; Rate constant; var. concentration reagents;

DOI:10.1021/jo00376a004

Reference yield:

N,N-dimethyl-aniline (121-69-7,77733-26-7) + p-tert-butylbenzenediazonium hexafluorophosphate (73286-45-0) → 4-tert-butyl-4'-(dimethylamino)azobenzene (24596-41-6)

Guidance literature:

In 1,2-dichloro-ethane; at 25 ℃; Rate constant;

DOI:10.1021/jo01298a065

Reference yield:

→ 4-tert-butyl-4'-(dimethylamino)azobenzene (24596-41-6)

Guidance literature:

/BRN= 658323/;

DOI:10.1021/jo01375a019

upstream raw materials:

N,N-dimethyl-aniline

p-tert-butylbenzenediazonium hexafluorophosphate

(4-tert-butylphenyl)diazonium tetrafluoroborate

Refernces

• 1、 Juri, Pedro N.,Bartsch, Richard A.. "Ion Pairing of Arenediazonium Salts in Solvents of Low Polarity". . p. 2028 - 2030. Retrieved 1980.